(E)-Methyl 2-(2-Methoxy-5-((2′,4′,6′-triMethoxystyrylsulfonyl)Methyl)phenylaMino)acetate

Base Information

Chemical Name:(E)-Methyl 2-(2-Methoxy-5-((2′,4′,6′-triMethoxystyrylsulfonyl)Methyl)phenylaMino)acetate
CAS No.:592542-61-5
Molecular Formula:C22H27NO8S
Molecular Weight:465.524
Hs Code.:
Mol file:592542-61-5.mol

Synonyms:methyl-{N-[2-methoxy-5-methylene(2',4',6'-trimethoxystyrylsulfonyl)-phenyl]amino}acetate;(E)-2,4,6-trimethoxystyryl-3-(carbomethoxymethylamino)-4-methoxybenzyl-sulfone;methyl (E)-2-(5-((2,4,6-trimethoxystyrylsulfonyl)methyl)-2-methoxyphenylamino)acetate;methyl 2-(5-((2,4,6-trimethoxystyrylsulfonyl)methyl)-2-methoxyphenylamino)acetate;(E)-2,4,6-trimethoxystyryl 3-(carbomethoxymethylamno)-4-methoxybenzyl-sulfone;

Suppliers and Price of (E)-Methyl 2-(2-Methoxy-5-((2′,4′,6′-triMethoxystyrylsulfonyl)Methyl)phenylaMino)acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

ChemScene
(E)-2,4,6-Trimethoxystyryl3-(carbomethoxymethylamino)-4-methoxybenzylsulfone
100mg
$ 500.00

Total 7 raw suppliers

Chemical Property of (E)-Methyl 2-(2-Methoxy-5-((2′,4′,6′-triMethoxystyrylsulfonyl)Methyl)phenylaMino)acetate

Chemical Property:

PSA：117.77000
LogP:4.04540

Purity/Quality:

97% ^*data from raw suppliers

(E)-2,4,6-Trimethoxystyryl3-(carbomethoxymethylamino)-4-methoxybenzylsulfone ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (E)-Methyl 2-(2-Methoxy-5-((2′,4′,6′-triMethoxystyrylsulfonyl)Methyl)phenylaMino)acetate

There total 14 articles about (E)-Methyl 2-(2-Methoxy-5-((2′,4′,6′-triMethoxystyrylsulfonyl)Methyl)phenylaMino)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 592542-50-2
(E)-2-methoxy-5-(((2,4,6-trimethoxystyryl)sulfonyl)methyl)aniline

: 96-32-2
bromoacetic acid methyl ester

: 592542-61-5
(E)-methyl 2-(2-methoxy-5-((2',4',6'-trimethoxystyrylsulfonyl)methyl)phenylamino)acetate

Guidance literature:: With sodium acetate; In methanol; Product distribution / selectivity; Heating / reflux;

Reference yield:

: (E)-2',4',6'-trimethoxystyryl-4-methoxy-3-nitrobenzylsulfone

: 592542-61-5
(E)-methyl 2-(2-methoxy-5-((2',4',6'-trimethoxystyrylsulfonyl)methyl)phenylamino)acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium dithionite / water; acetone / 1 h / 50 °C / Inert atmosphere

2.1: sodium acetate / methanol / 0.17 h / Inert atmosphere; Reflux

2.2: Inert atmosphere; Reflux

With sodium dithionite; sodium acetate; In methanol; water; acetone;
DOI:10.1021/jm200570p

Reference yield:

: 1330633-86-7
(E)-2',4',6'-trimethoxystyryl-4-methoxy-3-nitrobenzyl sulfide

: 592542-61-5
(E)-methyl 2-(2-methoxy-5-((2',4',6'-trimethoxystyrylsulfonyl)methyl)phenylamino)acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium dithionite / water; acetone / 1 h / 50 °C / Inert atmosphere

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

3.1: sodium acetate / methanol / 0.17 h / Inert atmosphere; Reflux

3.2: Inert atmosphere; Reflux

With sodium dithionite; sodium acetate; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane; water; acetone;
DOI:10.1021/jm200570p