2-(Bromomethyl)-2-(3-bromophenyl)-1,3-dioxolane

Base Information

Chemical Name:2-(Bromomethyl)-2-(3-bromophenyl)-1,3-dioxolane
CAS No.:60208-08-4
Molecular Formula:C10H10Br2O2
Molecular Weight:321.996
Hs Code.:
DSSTox Substance ID:DTXSID30504667
Nikkaji Number:J3.468.855I
Wikidata:Q82359323

Synonyms:60208-08-4;2-(Bromomethyl)-2-(3-bromophenyl)-1,3-dioxolane;SCHEMBL11465239;DTXSID30504667

Suppliers and Price of 2-(Bromomethyl)-2-(3-bromophenyl)-1,3-dioxolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 0 raw suppliers

Chemical Property of 2-(Bromomethyl)-2-(3-bromophenyl)-1,3-dioxolane

Chemical Property:

Melting Point:54-55 °C
Boiling Point:362.8±42.0 °C(Predicted)
PSA：18.46000
Density:1.751±0.06 g/cm3(Predicted)
LogP:3.04360
XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:321.90271
Heavy Atom Count:14
Complexity:193

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1COC(O1)(CBr)C2=CC(=CC=C2)Br

Technology Process of 2-(Bromomethyl)-2-(3-bromophenyl)-1,3-dioxolane

There total 2 articles about 2-(Bromomethyl)-2-(3-bromophenyl)-1,3-dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 107-21-1
ethylene glycol

: 18523-22-3
2,3'-dibromoacetophenone

: 60208-08-4
2-(bromomethyl)-2-(3-bromophenyl)-1,3-dioxolane

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 16h; Reflux;
DOI:10.1002/cmdc.201000120

Reference yield: 93.0%

: 107-21-1
ethylene glycol

: 2142-63-4
1-(3-Bromophenyl)ethanone

: 60208-08-4
2-(bromomethyl)-2-(3-bromophenyl)-1,3-dioxolane

Guidance literature:: With N-Bromosuccinimide; at 20 ℃; for 24h;
DOI:10.1016/j.tet.2016.05.064

Reference yield: 51.0%

: 288-32-4
1H-imidazole

: 60208-08-4
2-(bromomethyl)-2-(3-bromophenyl)-1,3-dioxolane

: 1353586-09-0
1-{[2-(3-bromophenyl)-1,3-dioxolan-2-yl]methyl}-1H-imidazole hydrochloride

Guidance literature:: 1H-imidazole; With sodium hydroxide; In dimethyl sulfoxide; at 60 - 70 ℃; for 1h;

2-(bromomethyl)-2-(3-bromophenyl)-1,3-dioxolane; In dimethyl sulfoxide; at 60 - 80 ℃;

With hydrogenchloride; In water; isopropyl alcohol;
DOI:10.1002/cmdc.201000120