2,6-Pyridinedimethanol

Base Information

• Chemical Name: 2,6-Pyridinedimethanol
• CAS No.: 1195-59-1
• Molecular Formula: C7H9NO2
• Molecular Weight: 139.154
• Hs Code.: 29333999
• European Community (EC) Number: 214-803-0
• NSC Number: 16571
• DSSTox Substance ID: DTXSID20152474
• Nikkaji Number: J41.162K
• Wikidata: Q72503913
• Mol file: 1195-59-1.mol

Synonyms:2,6-pyridinedimethanol

Chemical Property of 2,6-Pyridinedimethanol

Chemical Property:

• Appearance/Colour: light yellow to beige crystalline powder
• Vapor Pressure: 0.000574mmHg at 25°C
• Melting Point: 112-115 °C
• Refractive Index: 1.59
• Boiling Point: 298.3 °C at 760 mmHg
• PKA: 13.03±0.10(Predicted)
• Flash Point: 134.2 °C
• PSA: 53.35000
• Density: 1.261 g/cm³
• LogP: 0.06620
• Storage Temp.: Room temperature.
• Water Solubility.: Soluble in water.
• XLogP3: -0.8
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 139.063328530
• Heavy Atom Count: 10
• Complexity: 87.6

Purity/Quality:

99%, ^*data from raw suppliers

2,6-Pyridinedimethanol 98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 37/38-41-36/37/38
• Safety Statements: 26-39-24/25-36

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: C1=CC(=NC(=C1)CO)CO
• Uses: 2,6-Pyridinedimethanol can be used as a quantum dot solution for photoelectric device and biomedicine and also?a ligand to synthesize a variety of metal complexes and catalysts.

Technology Process of 2,6-Pyridinedimethanol

There total 18 articles about 2,6-Pyridinedimethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2,6-bis(methoxycarbonyl)pyridine (5453-67-8) → 2.6-bis(hydroxymethyl)pyridine (1195-59-1)

Guidance literature:

With sodium tetrahydroborate; In methanol;

DOI:10.1021/ol100749m

Reference yield: 94.5%

diethyl-2,6-pyridinedicarbonyl ester (15658-60-3) → 2.6-bis(hydroxymethyl)pyridine (1195-59-1)

Guidance literature:

With methanol; sodium tetrahydroborate; for 3h;

Reference yield: 90.5%

2,6-Pyridinedicarboxaldehyde (5431-44-7) → 2.6-bis(hydroxymethyl)pyridine (1195-59-1)

Guidance literature:

With sodium tetrahydroborate; In methanol; 1) 0 deg C, 0.5 h, 2) reflux, 1 h;

upstream raw materials:

2,6-Pyridinedicarboxaldehyde

diethyl-2,6-pyridinedicarbonyl ester

2,6-bis-acetoxymethyl-pyridine

2,6-bis(chloromethyl)pyridine

Downstream raw materials:

6-(hydroxymethyl)picolinaldehyde

2,6-bis(chloromethyl)pyridine

2,6-bis-(bromomethyl)pyridine

2-(4,4'-dimethoxytrityloxymethyl)-6-(hydroxymethyl)pyridine

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