2-Iodo-1-phenylnaphthalene

Base Information

• Chemical Name: 2-Iodo-1-phenylnaphthalene
• CAS No.: 607731-70-4
• Molecular Formula: C16H11I
• Molecular Weight: 330.168
• DSSTox Substance ID: DTXSID40457756
• Nikkaji Number: J1.957.620E
• Wikidata: Q82280734
• Mol file: 607731-70-4.mol

Synonyms:2-IODO-1-PHENYLNAPHTHALENE;607731-70-4;Naphthalene, 2-iodo-1-phenyl-;1-Phenyl-2-iodonaphthalene;SCHEMBL12695622;DTXSID40457756;KUC100626N;AKOS015966126

Chemical Property of 2-Iodo-1-phenylnaphthalene

Chemical Property:

• XLogP3: 5.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 1
• Exact Mass: 329.99055
• Heavy Atom Count: 17
• Complexity: 244

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C2=C(C=CC3=CC=CC=C32)I

Technology Process of 2-Iodo-1-phenylnaphthalene

There total 10 articles about 2-Iodo-1-phenylnaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

1,4-diphenyl-3-butyn-2-ol (62969-97-5) → 2-iodo-1-phenylnaphthalene (607731-70-4)

Guidance literature:

With Iodine monochloride; sodium hydrogencarbonate; In acetonitrile; at 20 ℃; for 0.0833333h;

DOI:10.1021/jo051948k

Reference yield: 70.0%

1-phenyl-3,4-dihydronaphthalene (7469-40-1) → 2-iodo-1-phenylnaphthalene (607731-70-4)

Guidance literature:

1-phenyl-3,4-dihydronaphthalene; With iodine; silver trifluoromethanesulfonate; In acetonitrile; at 20 ℃; for 1h;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In benzene; at 65 ℃; for 48h;

DOI:10.1021/ja035121o

Reference yield: 51.0%

1-benzyl-3-phenylprop-2-ynyl acetate (874338-64-4) → 2-iodo-1-phenylnaphthalene (607731-70-4)

Guidance literature:

With iodine; sodium hydrogencarbonate; In acetonitrile; at 20 ℃;

DOI:10.1021/jo051948k

upstream raw materials:

1-phenyl-3,4-dihydronaphthalene

1-benzyl-3-phenylprop-2-ynyl acetate

1,4-diphenyl-3-butyn-2-ol

1,4-diphenylbut-3-yn-1-ol

Downstream raw materials:

fluoranthene

2-[(4-methoxyphenyl)ethynyl]-1-phenylnaphthalene