9,10-Dihydrotetraphen-11(8H)-one

Base Information

Chemical Name:9,10-Dihydrotetraphen-11(8H)-one
CAS No.:60968-15-2
Molecular Formula:C18H14O
Molecular Weight:246.309
Hs Code.:
DSSTox Substance ID:DTXSID20491057
Wikidata:Q82335235

Synonyms:60968-15-2;9,10-dihydro-8H-benzo[a]anthracen-11-one;9,10-Dihydrobenz[a]anthracen-11(8H)-one;9,10-Dihydrotetraphen-11(8H)-one;DTXSID20491057;AKOS030255063;9,10-Dihydro-benz[a]anthracen-11(8)-one

Suppliers and Price of 9,10-Dihydrotetraphen-11(8H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9,10-Dihydrotetraphen-11(8H)-one

Chemical Property:

XLogP3:4.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:246.104465066
Heavy Atom Count:19
Complexity:361

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC2=C(C=C3C(=C2)C=CC4=CC=CC=C43)C(=O)C1

Technology Process of 9,10-Dihydrotetraphen-11(8H)-one

There total 1 articles about 9,10-Dihydrotetraphen-11(8H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 67064-62-4
8,9,10,11-tetrahydro-benzo[a]anthracene

: 56-55-3
benz[a]anthracene

: 60968-15-2
8,9,10,11-tetrahydrobenz anthracen-11-one

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In water; acetic acid; for 0.666667h; Heating;
DOI:10.1021/jo00254a035

Reference yield:

: 60968-15-2
8,9,10,11-tetrahydrobenz anthracen-11-one

: 60967-90-0
trans-10,11-dihydroxy-10,11-dihydrobenz anthracene

Guidance literature:: Multi-step reaction with 5 steps

1: (i) NaBH₄, (ii) aq. HCl

2: I₂

3: NBS, AIBN

4: NaHCO₃

5: NaOMe

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); iodine; sodium methylate; sodium hydrogencarbonate;
DOI:10.1021/jo00424a036