[(Cyanocarbonyl)(phenyl)amino]benzene

Base Information

Chemical Name:[(Cyanocarbonyl)(phenyl)amino]benzene
CAS No.:61097-42-5
Molecular Formula:C14H10N2O
Molecular Weight:222.246
Hs Code.:
DSSTox Substance ID:DTXSID70493980
Nikkaji Number:J3.134.484K
Wikidata:Q82341011

Synonyms:[(Cyanocarbonyl)(phenyl)amino]benzene;61097-42-5;SCHEMBL11862805;DTXSID70493980

Suppliers and Price of [(Cyanocarbonyl)(phenyl)amino]benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [(Cyanocarbonyl)(phenyl)amino]benzene

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:222.079312947
Heavy Atom Count:17
Complexity:287

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)N(C2=CC=CC=C2)C(=O)C#N

Technology Process of [(Cyanocarbonyl)(phenyl)amino]benzene

There total 7 articles about [(Cyanocarbonyl)(phenyl)amino]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 3,3,3-trifluoro-N,N-diphenylpropanamide

: 61097-42-5
diphenylcarbamoyl cyanide

Guidance literature:: With tert.-butylnitrite; caesium carbonate; acetic acid; In acetonitrile; at 100 ℃; for 24h; Schlenk technique; Molecular sieve;
DOI:10.1021/acs.joc.7b00626

Reference yield: 9.0%

: 122-39-4
diphenylamine

: 545-06-2
trichloroacetonitrile

: 61097-42-5
diphenylcarbamoyl cyanide

Guidance literature:: With tetrabutylammonium perchlorate; C₅₁H₇₁CoN₄O₁₄; In acetonitrile; at 20 ℃; for 1.5h; Electrolysis;
DOI:10.1021/acs.joc.1c00837

Reference yield:

: 122-39-4
diphenylamine

: 61097-42-5
diphenylcarbamoyl cyanide

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / dichloromethane / 0.25 h / -30 °C / Inert atmosphere; Schlenk technique

1.2: 6 h / -30 - 20 °C / Inert atmosphere; Schlenk technique

2.1: acetonitrile / 75 °C

With pyridine; In dichloromethane; acetonitrile;
DOI:10.1002/chem.201202607