Benzene, 1,5-bis(chloromethyl)-2,4-diethyl-

Base Information

Chemical Name:Benzene, 1,5-bis(chloromethyl)-2,4-diethyl-
CAS No.:61099-13-6
Molecular Formula:C12H16Cl2
Molecular Weight:231.165
Hs Code.:
DSSTox Substance ID:DTXSID90356760
Wikidata:Q82136319

Synonyms:61099-13-6;Benzene, 1,5-bis(chloromethyl)-2,4-diethyl-;DTXSID90356760

Suppliers and Price of Benzene, 1,5-bis(chloromethyl)-2,4-diethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzene, 1,5-bis(chloromethyl)-2,4-diethyl-

Chemical Property:

XLogP3:4.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:4
Exact Mass:230.0629059
Heavy Atom Count:14
Complexity:142

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC1=CC(=C(C=C1CCl)CCl)CC

Technology Process of Benzene, 1,5-bis(chloromethyl)-2,4-diethyl-

There total 1 articles about Benzene, 1,5-bis(chloromethyl)-2,4-diethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 141-93-5
m-diethylbenzene

: 61099-13-6
4,6-Bis(chlormethyl)-m-diethylbenzol

Guidance literature:: With hydrogenchloride; zinc(II) chloride; In tetrachloromethane;
DOI:10.1039/P29760001195

Reference yield: 76.0%

: 61099-13-6
4,6-Bis(chlormethyl)-m-diethylbenzol

: C₅H₁₆BP

: (S,S)-1,5-bis((borane-tert-butylmethylphosphino)methylene)-2,4-diethylbenzene

Guidance literature:: C₅H₁₆BP; With n-butyllithium; In tetrahydrofuran; hexane; at -80 ℃; for 0.5h;

4,6-Bis(chlormethyl)-m-diethylbenzol; In tetrahydrofuran; hexane; at 20 ℃;

Reference yield:

: 61099-13-6
4,6-Bis(chlormethyl)-m-diethylbenzol

: C₅H₁₆BP

: (S,S)-1,5-bis((tert-butylmethylphosphino)methylene)-2,4-diethylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -80 °C

1.2: 20 °C

2.1: trifluorormethanesulfonic acid / toluene / 1.5 h / 0 - 20 °C

With n-butyllithium; trifluorormethanesulfonic acid; In tetrahydrofuran; hexane; toluene;