1,1-Cyclopropanedicarboxylic acid, 2-(1-methylethenyl)-, dimethyl ester

Base Information

Chemical Name:1,1-Cyclopropanedicarboxylic acid, 2-(1-methylethenyl)-, dimethyl ester
CAS No.:61111-65-7
Molecular Formula:C10H14O4
Molecular Weight:198.219
Hs Code.:

Synonyms:dimethyl 2-isopropenylcyclopropane-1,1-dicarboxylate;dimethyl 2-isopropenyl-1,1-cyclopropanedicarboxylate;1,1-Cyclopropanedicarboxylic acid,2-(1-methylethenyl)-,dimethyl ester;dimethyl 2-(1-methylethenyl)cyclopropane-1,1-dicarboxylate;<2RS>-2-Isopropenylcyclopropan-1,1-dicarbonsaeure-dimethylester;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1-Cyclopropanedicarboxylic acid, 2-(1-methylethenyl)-, dimethyl ester

Chemical Property:

Boiling Point:105-107 °C(Press: 10 Torr)
PSA：52.60000
Density:1.149±0.06 g/cm3(Predicted)
LogP:0.91480

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,1-Cyclopropanedicarboxylic acid, 2-(1-methylethenyl)-, dimethyl ester

There total 1 articles about 1,1-Cyclopropanedicarboxylic acid, 2-(1-methylethenyl)-, dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 18860-95-2
1,4-dibromo-2-methylbut-2-ene

: 108-59-8
malonic acid dimethyl ester

: 61111-66-8
dimethyl 2-vinyl-2-methyl-1,1-cyclopropanedicarboxylate

: 61111-65-7
<2RS>-2-Isopropenylcyclopropan-1,1-dicarbonsaeure-dimethylester

Guidance literature:: With N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate; In acetonitrile; for 8h; Heating;

Reference yield: 90.0%

: 61111-65-7
<2RS>-2-Isopropenylcyclopropan-1,1-dicarbonsaeure-dimethylester

: 103-71-9
phenyl isocyanate

: 112723-45-2
5-Isopropenyl-2-oxo-1-phenyl-pyrrolidine-3,3-dicarboxylic acid dimethyl ester

Guidance literature:: With tributylphosphine; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 25 ℃; for 15h;
DOI:10.1246/cl.1987.1157

Reference yield:

: 61111-65-7
<2RS>-2-Isopropenylcyclopropan-1,1-dicarbonsaeure-dimethylester

: 103259-99-0
(S)-2-Isopropenyl-cyclopropane-1,1-dicarboxylic acid; compound with (S)-1-phenyl-ethylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 66 percent / KOH / H₂O / 16 h / Ambient temperature

3: 82 percent / diethyl ether / 16 h / Ambient temperature

With potassium hydroxide; In diethyl ether; water;