Technology Process of Benzoic acid,
2-hydroxy-4-[[2-hydroxy-6-methyl-4-(phenylmethoxy)benzoyl]oxy]-6-meth
yl-, methyl ester
There total 1 articles about Benzoic acid,
2-hydroxy-4-[[2-hydroxy-6-methyl-4-(phenylmethoxy)benzoyl]oxy]-6-meth
yl-, methyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
4-Benzyloxy-2-hydroxy-6-methylbenzoesaeure (8), Methyl-orsellinat (9), (CF3CO)2O, Toluol;
- Guidance literature:
-
With
potassium carbonate;
In
dimethyl sulfoxide;
for 12h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 87 percent / potassium carbonate / dimethylsulfoxide / 2 h / Ambient temperature
2: 97 percent / H2 / 10percent Pd/C / ethyl acetate / 2 h
3: 60 percent / ethyl acetate / 0.08 h / Ambient temperature
4: 90 percent / potassium carbonate / acetone / 27 h / Heating
With
hydrogen; potassium carbonate;
palladium on activated charcoal;
In
dimethyl sulfoxide; ethyl acetate; acetone;
