3,9-Dimethoxy-1,7-dimethyl-2,6-dibenzofurandicarboxylic acid 2-methyl ester

Base Information

Chemical Name:3,9-Dimethoxy-1,7-dimethyl-2,6-dibenzofurandicarboxylic acid 2-methyl ester
CAS No.:27161-92-8
Molecular Formula:C₁₉H₁₈O₇
Molecular Weight:358.348
Hs Code.:
Mol file:27161-92-8.mol

Synonyms:Schizopelticacid

Suppliers and Price of 3,9-Dimethoxy-1,7-dimethyl-2,6-dibenzofurandicarboxylic acid 2-methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 3,9-Dimethoxy-1,7-dimethyl-2,6-dibenzofurandicarboxylic acid 2-methyl ester

Chemical Property:

Melting Point:229-231 °C (decomp)
Boiling Point:549.9±45.0 °C(Predicted)
PKA:3.07±0.30(Predicted)
PSA：95.20000
Density:1.320±0.06 g/cm3(Predicted)
LogP:3.70480

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3,9-Dimethoxy-1,7-dimethyl-2,6-dibenzofurandicarboxylic acid 2-methyl ester

There total 23 articles about 3,9-Dimethoxy-1,7-dimethyl-2,6-dibenzofurandicarboxylic acid 2-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 84161-45-5
benzyl schizopeltate

: 27161-92-8
schizopeltic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 2h;

Reference yield:

: 61158-11-0
methyl 4-O-benzyllecanorate

: 27161-92-8
schizopeltic acid

Guidance literature:: Multi-step reaction with 6 steps

1: 87 percent / potassium carbonate / dimethylsulfoxide / 2 h / Ambient temperature

2: 97 percent / H₂ / 10percent Pd/C / ethyl acetate / 2 h

3: 60 percent / ethyl acetate / 0.08 h / Ambient temperature

4: 90 percent / potassium carbonate / acetone / 27 h / Heating

5: 58 percent / palladium acetate, trifluoroacetic acid / acetic acid / 4.5 h / Ambient temperature

6: 97 percent / H₂ / 10percent Pd/C / ethyl acetate / 2 h

With hydrogen; palladium diacetate; potassium carbonate; trifluoroacetic acid; palladium on activated charcoal; In acetic acid; dimethyl sulfoxide; ethyl acetate; acetone;

Reference yield:

: 111699-18-4
4-benzyloxy-2-(3'-hydroxy-4'-methoxycarbonyl-5'-methylphenoxy)-6-methylbenzoic acid

: 27161-92-8
schizopeltic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / H₂ / 10percent Pd/C / ethyl acetate / 2 h

2: 60 percent / ethyl acetate / 0.08 h / Ambient temperature

3: 90 percent / potassium carbonate / acetone / 27 h / Heating

4: 58 percent / palladium acetate, trifluoroacetic acid / acetic acid / 4.5 h / Ambient temperature

5: 97 percent / H₂ / 10percent Pd/C / ethyl acetate / 2 h

With hydrogen; palladium diacetate; potassium carbonate; trifluoroacetic acid; palladium on activated charcoal; In acetic acid; ethyl acetate; acetone;