Phosphine oxide, diphenyl[1-(phenylthio)propyl]-

Base Information

Chemical Name:Phosphine oxide, diphenyl[1-(phenylthio)propyl]-
CAS No.:61173-97-5
Molecular Formula:C21H21OPS
Molecular Weight:352.437
Hs Code.:
DSSTox Substance ID:DTXSID80486222

Synonyms:Phosphine oxide, diphenyl[1-(phenylthio)propyl]-;61173-97-5;DTXSID80486222

Suppliers and Price of Phosphine oxide, diphenyl[1-(phenylthio)propyl]-

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Chemical Property of Phosphine oxide, diphenyl[1-(phenylthio)propyl]-

Chemical Property:

XLogP3:5.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:6
Exact Mass:352.10507346
Heavy Atom Count:24
Complexity:384

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCC(P(=O)(C1=CC=CC=C1)C2=CC=CC=C2)SC3=CC=CC=C3

Technology Process of Phosphine oxide, diphenyl[1-(phenylthio)propyl]-

There total 8 articles about Phosphine oxide, diphenyl[1-(phenylthio)propyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 917-54-4
methyllithium

: 84904-72-3
Diphenyl (1-phenylthiovinyl)phosphine oxide

: 61173-97-5
1-phenylthiopropyldiphenylphosphine oxide

Guidance literature:: In tetrahydrofuran; diethyl ether; at -78 ℃; for 0.166667h;

Reference yield:

: 66164-48-5
diphenyl(1-(phenylthio)ethyl)phosphine oxide

: 61173-97-5
1-phenylthiopropyldiphenylphosphine oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 1) NCS, 2) silica gel / 1) CCl₄, 50 deg C, 4.5 h, 2) EtOAc, 16 h

2: 71 percent / diethyl ether; tetrahydrofuran / 0.17 h / -78 °C

With N-chloro-succinimide; silica gel; In tetrahydrofuran; diethyl ether;

Reference yield:

: 84904-74-5
1-phenylsulphinylethyldiphenylphosphine oxide

: 61173-97-5
1-phenylthiopropyldiphenylphosphine oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / Ac₂O, MeSO₃H / CH₂Cl₂ / 192 h / Ambient temperature

2: 71 percent / diethyl ether; tetrahydrofuran / 0.17 h / -78 °C

With methanesulfonic acid; acetic anhydride; In tetrahydrofuran; diethyl ether; dichloromethane;