Benzene, 1-methyl-2-[(2-nitrophenyl)sulfonyl]-

Base Information

Chemical Name:Benzene, 1-methyl-2-[(2-nitrophenyl)sulfonyl]-
CAS No.:61174-13-8
Molecular Formula:C13H11NO4S
Molecular Weight:277.29600
Hs Code.:
European Community (EC) Number:660-294-7
DSSTox Substance ID:DTXSID30393235
Wikidata:Q82191919

Synonyms:61174-13-8;Benzene, 1-methyl-2-[(2-nitrophenyl)sulfonyl]-;1-methyl-2-(2-nitrophenyl)sulfonylbenzene;DTXSID30393235;2-methylphenyl 2-nitrophenyl sulfone;AKOS024338860

Suppliers and Price of Benzene, 1-methyl-2-[(2-nitrophenyl)sulfonyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
2-NITROPHENYL O-TOLYL SULFONE Aldrich
1ea
$ 57.00

Total 0 raw suppliers

Chemical Property of Benzene, 1-methyl-2-[(2-nitrophenyl)sulfonyl]-

Chemical Property:

PSA：88.34000
LogP:4.34000
XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:277.04087901
Heavy Atom Count:19
Complexity:423

Purity/Quality:: 2-NITROPHENYL O-TOLYL SULFONE Aldrich ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=CC=C1S(=O)(=O)C2=CC=CC=C2[N+](=O)[O-]

Technology Process of Benzene, 1-methyl-2-[(2-nitrophenyl)sulfonyl]-

There total 5 articles about Benzene, 1-methyl-2-[(2-nitrophenyl)sulfonyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 552-16-9,104810-18-6
ortho-nitrobenzoic acid

: 15898-37-0
sodium 2-methylbenzenesulfinate

: 61174-13-8
1-methyl-2-((2-nitrophenyl)sulfonyl)benzene

Guidance literature:: With 1,10-Phenanthroline; silver carbonate; at 160 ℃; for 18h; Schlenk technique; Sealed tube;
DOI:10.1021/acs.joc.9b01333

Reference yield:

: 6640-54-6
(2-methylphenyl)-(2-nitrophenyl)thioether

: 61174-13-8
1-methyl-2-((2-nitrophenyl)sulfonyl)benzene

Guidance literature:: With dihydrogen peroxide; acetic acid; Erhitzen auf dem Dampfbad;
DOI:10.1021/ja01200a069

Reference yield:

: 88-73-3
2-Chloronitrobenzene

: 61174-13-8
1-methyl-2-((2-nitrophenyl)sulfonyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: KOH / ethanol / Heating

2: H₂O₂ / acetic acid

With potassium hydroxide; dihydrogen peroxide; In ethanol; acetic acid;
DOI:10.1016/0022-2860(91)85080-M