2,4-Dithia-6,8-diazabicyclo[3.2.2]nonane-7,9-dione, 6-[6-(acetyloxy)-2-(hydroxymethyl)-2,4-cyclohexadien-1-yl]-3-(4-methoxy phenyl)-8-methyl-

Base Information

Chemical Name:2,4-Dithia-6,8-diazabicyclo[3.2.2]nonane-7,9-dione, 6-[6-(acetyloxy)-2-(hydroxymethyl)-2,4-cyclohexadien-1-yl]-3-(4-methoxy phenyl)-8-methyl-
CAS No.:61377-99-9
Molecular Formula:C₂₂H₂₄N₂O₆S₂
Molecular Weight:476.574
Hs Code.:

2,4-Dithia-6,8-diazabicyclo[3.2.2]nonane-7,9-dione,
6-[6-(acetyloxy)-2-(hydroxymethyl)-2,4-cyclohexadien-1-yl]-3-(4-methoxy
phenyl)-8-methyl-

Synonyms:

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Chemical Property of 2,4-Dithia-6,8-diazabicyclo[3.2.2]nonane-7,9-dione, 6-[6-(acetyloxy)-2-(hydroxymethyl)-2,4-cyclohexadien-1-yl]-3-(4-methoxy phenyl)-8-methyl-

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Technology Process of 2,4-Dithia-6,8-diazabicyclo[3.2.2]nonane-7,9-dione, 6-[6-(acetyloxy)-2-(hydroxymethyl)-2,4-cyclohexadien-1-yl]-3-(4-methoxy phenyl)-8-methyl-

There total 21 articles about 2,4-Dithia-6,8-diazabicyclo[3.2.2]nonane-7,9-dione, 6-[6-(acetyloxy)-2-(hydroxymethyl)-2,4-cyclohexadien-1-yl]-3-(4-methoxy phenyl)-8-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Acetic acid (1S,6S)-5-ethoxycarbonyloxycarbonyl-6-[(1R,3S,5R)-3-(4-methoxy-phenyl)-8-methyl-7,9-dioxo-2,4-dithia-6,8-diaza-bicyclo[3.2.2]non-6-yl]-cyclohexa-2,4-dienyl ester

: 61377-99-9,79355-31-0,79355-32-1
Acetic acid (1S,6S)-5-hydroxymethyl-6-[(1R,3S,5R)-3-(4-methoxy-phenyl)-8-methyl-7,9-dioxo-2,4-dithia-6,8-diaza-bicyclo[3.2.2]non-6-yl]-cyclohexa-2,4-dienyl ester

Guidance literature:: With sodium tetrahydroborate; In methanol; dichloromethane; at 0 ℃; for 0.166667h; Yield given;
DOI:10.1016/S0040-4020(01)97960-8

Reference yield:

: Acetic acid (1S,6S)-5-ethoxycarbonyloxycarbonyl-6-[(1R,3R,5R)-3-(4-methoxy-phenyl)-8-methyl-7,9-dioxo-2,4-dithia-6,8-diaza-bicyclo[3.2.2]non-6-yl]-cyclohexa-2,4-dienyl ester

: 61377-99-9,79355-31-0,79355-32-1
Acetic acid (1S,6S)-5-hydroxymethyl-6-[(1R,3R,5R)-3-(4-methoxy-phenyl)-8-methyl-7,9-dioxo-2,4-dithia-6,8-diaza-bicyclo[3.2.2]non-6-yl]-cyclohexa-2,4-dienyl ester

Guidance literature:: With sodium tetrahydroborate; In methanol; dichloromethane; at 0 ℃; for 0.166667h; Yield given;
DOI:10.1016/S0040-4020(01)97960-8

Reference yield:

: Acetic acid (1S,6S)-5-ethoxycarbonyloxycarbonyl-6-[(1R,3S,5R)-3-(4-methoxy-phenyl)-8-methyl-7,9-dioxo-2,4-dithia-6,8-diaza-bicyclo[3.2.2]non-6-yl]-cyclohexa-2,4-dienyl ester

: 61377-99-9,79355-31-0,79355-32-1
Acetic acid (1S,6S)-5-hydroxymethyl-6-[(1R,3S,5R)-3-(4-methoxy-phenyl)-8-methyl-7,9-dioxo-2,4-dithia-6,8-diaza-bicyclo[3.2.2]non-6-yl]-cyclohexa-2,4-dienyl ester

Guidance literature:: With sodium tetrahydroborate; In methanol; dichloromethane; at 0 ℃; for 0.166667h; Yield given;
DOI:10.1016/S0040-4020(01)97960-8