Technology Process of Phosphine oxide, ethylphenylpropyl-
There total 5 articles about Phosphine oxide, ethylphenylpropyl- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
propyl bromide;
With
magnesium;
In
tetrahydrofuran;
Inert atmosphere;
Schlenk technique;
ethylphenylphosphinic acid ethyl ester;
With
toluene;
In
tetrahydrofuran;
at 0 - 60 ℃;
for 20h;
Inert atmosphere;
Schlenk technique;
DOI:10.1002/ejoc.202000035
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: pyridine / hexane / Inert atmosphere; Cooling with ice
1.2: 17 h / 0 - 26 °C / Inert atmosphere
2.1: 21.5 h / 26 - 80 °C / Inert atmosphere
3.1: magnesium / tetrahydrofuran / Inert atmosphere; Schlenk technique
3.2: 20 h / 0 - 60 °C / Inert atmosphere; Schlenk technique
With
pyridine; magnesium;
In
tetrahydrofuran; hexane;
DOI:10.1002/ejoc.202000035
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 21.5 h / 26 - 80 °C / Inert atmosphere
2.1: magnesium / tetrahydrofuran / Inert atmosphere; Schlenk technique
2.2: 20 h / 0 - 60 °C / Inert atmosphere; Schlenk technique
With
magnesium;
In
tetrahydrofuran;
DOI:10.1002/ejoc.202000035