2,5-Cyclohexadien-1-one, 2,6-dimethyl-4-(phenylmethylene)-

Base Information

Chemical Name:2,5-Cyclohexadien-1-one, 2,6-dimethyl-4-(phenylmethylene)-
CAS No.:61400-67-7
Molecular Formula:C15H14O
Molecular Weight:210.276
Hs Code.:

Synonyms:2,6-Dimethyl-4-benzylidene-2,5-cyclohexadien-1-on;2,6-Dimethyl-benzyliden-2,5-cyclohexadien-1-on;

Suppliers and Price of 2,5-Cyclohexadien-1-one, 2,6-dimethyl-4-(phenylmethylene)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,5-Cyclohexadien-1-one, 2,6-dimethyl-4-(phenylmethylene)-

Chemical Property:

Boiling Point:373.0±22.0 °C(Predicted)
PSA：17.07000
Density:1.087±0.06 g/cm3(Predicted)
LogP:3.54530

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,5-Cyclohexadien-1-one, 2,6-dimethyl-4-(phenylmethylene)-

There total 8 articles about 2,5-Cyclohexadien-1-one, 2,6-dimethyl-4-(phenylmethylene)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 41772-31-0
4‐benzyl‐2,6‐dimethylphenol

: 61400-67-7
4-phenylmethylene-2,6-dimethyl-2,5-cyclohexadien-1-one

Guidance literature:: With potassium hydroxide; potassium hexacyanoferrate(III); In n-heptane; water; for 2h; Inert atmosphere;
DOI:10.1021/acs.orglett.7b00869

Reference yield:

: 576-26-1,25134-01-4
2.6-dimethylphenol

: 100-52-7
benzaldehyde

: 61400-67-7
4-phenylmethylene-2,6-dimethyl-2,5-cyclohexadien-1-one

Guidance literature:: 2.6-dimethylphenol; benzaldehyde; With piperidine; In toluene; for 3h; Reflux; Dean-Stark;

With acetic anhydride; In toluene; for 0.25h; Heating;
DOI:10.1055/s-0036-1588546

Reference yield:

: 98-88-4
benzoyl chloride

: 61400-67-7
4-phenylmethylene-2,6-dimethyl-2,5-cyclohexadien-1-one

Guidance literature:: Multi-step reaction with 3 steps

1: aluminum (III) chloride / toluene / 7 h / 20 °C

2: palladium on activated carbon; hydrogen / ethanol / 3 h / 23 °C

3: potassium hydroxide; potassium hexacyanoferrate(III) / water; hexane / 1 h / 23 °C / Inert atmosphere

With aluminum (III) chloride; palladium on activated carbon; hydrogen; potassium hydroxide; potassium hexacyanoferrate(III); In ethanol; hexane; water; toluene;
DOI:10.1039/c5cc06287j