4-nitro-1-N-phenylbenzene-1,2-diamine

Base Information

Chemical Name:4-nitro-1-N-phenylbenzene-1,2-diamine
CAS No.:55315-12-3
Molecular Formula:C12H11 N3 O2
Molecular Weight:229.238
Hs Code.:2921590090
NSC Number:157788
UNII:ACC2Z8RFT6
DSSTox Substance ID:DTXSID00203872
Nikkaji Number:J90.264K
Wikidata:Q83077299
Pharos Ligand ID:V31YVJ2JB3YN
ChEMBL ID:CHEMBL1492242
Mol file:55315-12-3.mol

Synonyms:55315-12-3;4-nitro-1-N-phenylbenzene-1,2-diamine;4-nitro-N1-phenylbenzene-1,2-diamine;N-(2-amino-4-nitrophenyl)-N-phenylamine;2-Phenylamino-5-nitroaniline;1,2-Phenylenediamine, 4-nitro-N1-phenyl-;(2-amino-4-nitrophenyl)phenylamine;ACC2Z8RFT6;4-nitro-N~1~-phenylbenzene-1,2-diamine;MLS000677553;NSC 157788;NSC-157788;SMR000271721;NSC157788;4-nitro-N1-phenyl-1,2-Benzenediamine;UNII-ACC2Z8RFT6;4-Nitro-2-amino-diphenylamin;SCHEMBL6582107;TQR946;CHEMBL1492242;BDBM94804;cid_3750424;2-Amino-4-nitro-N-phenylaniline;DTXSID00203872;HMS2611A23;MFCD00234791;STL497551;AKOS001393914;N-Phenyl-4-nitro-1,2-benzenediamine;(2-amino-4-nitro-phenyl)-phenyl-amine;4-nitro-N1-phenyl-benzene-1,2-diamine;NCGC00245654-01;CS-0220716;FT-0725916;EN300-07363;AC-907/25005196;SR-01000391667;SR-01000391667-1;Z56955918;F1196-0222

Suppliers and Price of 4-nitro-1-N-phenylbenzene-1,2-diamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
4-Nitro-1-N-phenylbenzene-1,2-diamine
50mg
$ 90.00

TRC
4-Nitro-1-N-phenylbenzene-1,2-diamine
250mg
$ 350.00

American Custom Chemicals Corporation
N-(2-AMINO-4-NITROPHENYL)-N-PHENYLAMINE 95.00%
2.5G
$ 1363.65

American Custom Chemicals Corporation
N-(2-AMINO-4-NITROPHENYL)-N-PHENYLAMINE 95.00%
1G
$ 925.31

American Custom Chemicals Corporation
N-(2-AMINO-4-NITROPHENYL)-N-PHENYLAMINE 95.00%
5G
$ 1759.28

AK Scientific
N-(2-Amino-4-nitrophenyl)-N-phenylamine
5g
$ 1606.00

AK Scientific
N-(2-Amino-4-nitrophenyl)-N-phenylamine
500mg
$ 483.00

AK Scientific
N-(2-Amino-4-nitrophenyl)-N-phenylamine
250mg
$ 301.00

Total 7 raw suppliers

Chemical Property of 4-nitro-1-N-phenylbenzene-1,2-diamine

Chemical Property:

Vapor Pressure:2.01E-07mmHg at 25°C
Boiling Point:424.8°C at 760 mmHg
Flash Point:210.7°C
PSA：83.87000
Density:1.351g/cm³
LogP:4.09800
XLogP3:2.6
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:229.085126602
Heavy Atom Count:17
Complexity:261

Purity/Quality:

98%+ ^*data from raw suppliers

4-Nitro-1-N-phenylbenzene-1,2-diamine ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)NC2=C(C=C(C=C2)[N+](=O)[O-])N

Technology Process of 4-nitro-1-N-phenylbenzene-1,2-diamine

There total 11 articles about 4-nitro-1-N-phenylbenzene-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 961-68-2
N-phenyl-2,4-dinitroaniline

: 55315-12-3
2-amino-4-nitro-N₁-phenylaniline

Guidance literature:: With sodium sulfide; water; sulfur; In ethanol; for 2h; Reflux;
DOI:10.1021/acs.inorgchem.9b01678

Reference yield: 29.0%

: 961-68-2
N-phenyl-2,4-dinitroaniline

: 2784-89-6
1-anilino-4-amino-2-nitrobenzene

: 55315-12-3
2-amino-4-nitro-N₁-phenylaniline

Guidance literature:: With nickel; hydrazine hydrate; In ethanol; 1,2-dichloro-ethane; at 50 - 60 ℃; for 4h;
DOI:10.1246/bcsj.56.3159

Reference yield:

: 62-53-3
aniline

: 55315-12-3
2-amino-4-nitro-N₁-phenylaniline

Guidance literature:: Multi-step reaction with 2 steps

1: sodium acetate / ethanol / 1 h / 78 °C

2: sodium sulfide; sulfur; water / ethanol / 2 h / Reflux

With sodium sulfide; water; sodium acetate; sulfur; In ethanol;
DOI:10.1021/acs.inorgchem.9b01678