5-Nitro-1-phenylbenzimidazole

Base Information

Chemical Name:5-Nitro-1-phenylbenzimidazole
CAS No.:15127-88-5
Molecular Formula:C13H9N3O2
Molecular Weight:239.233
Hs Code.:
DSSTox Substance ID:DTXSID00353386
Wikidata:Q82130964
ChEMBL ID:CHEMBL153208
Mol file:15127-88-5.mol

Synonyms:5-nitro-1-phenylbenzimidazole;5-nitro-1-phenyl-1H-benzimidazole;15127-88-5;5-nitro-1-phenyl-1H-1,3-benzodiazole;MLS000553360;5-Nitro-1-phenyl-1H-benzoimidazole;Cambridge id 5659846;Oprea1_293142;Oprea1_793806;BDBM3853;CHEMBL153208;SCHEMBL3342620;1-Phenylbenzimidazole deriv. 70;DTXSID00353386;HMS2558A08;CCG-46050;MFCD00179556;STK003475;AKOS000562552;5-nitro-1-phenyl-1H-benzo[d]imidazole;LS-07572;SMR000175668;AB00092174-01;SR-01000439600;SR-01000439600-1;SR-01000439600-2

Suppliers and Price of 5-Nitro-1-phenylbenzimidazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
5-Nitro-1-phenyl-1H-benzo[d]imidazole 97%
5g
$ 527.00

Total 1 raw suppliers

Chemical Property of 5-Nitro-1-phenylbenzimidazole

Chemical Property:

Boiling Point:449.1±37.0 °C(Predicted)
PSA：63.64000
Density:1.34±0.1 g/cm3(Predicted)
LogP:3.45690
XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:239.069476538
Heavy Atom Count:18
Complexity:312

Purity/Quality:: 5-Nitro-1-phenyl-1H-benzo[d]imidazole 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)N2C=NC3=C2C=CC(=C3)[N+](=O)[O-]

Technology Process of 5-Nitro-1-phenylbenzimidazole

There total 16 articles about 5-Nitro-1-phenylbenzimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 64-18-6
formic acid

: 55315-12-3
2-amino-4-nitro-N₁-phenylaniline

: 15127-88-5
5-nitro-1-phenyl-1H-benzo[d]imidazole

Guidance literature:: at 100 ℃; for 12h;
DOI:10.1021/acs.inorgchem.9b01678

Reference yield: 89.0%

: 591-50-4
iodobenzene

: 94-52-0
5-nitrobenzimidazole

: 15127-88-5
5-nitro-1-phenyl-1H-benzo[d]imidazole

Guidance literature:: With copper(l) iodide; 2-(2-benzoylhydrazine-1-carbonyl)-1-benzylpyrrolidine 1-oxide; caesium carbonate; In ethanol; at 80 ℃; for 12h; Inert atmosphere; Sealed tube;
DOI:10.1016/j.tet.2020.131826

Reference yield: 64.0%

: 591-50-4
iodobenzene

: 94-52-0
5-nitrobenzimidazole

: 15127-88-5
5-nitro-1-phenyl-1H-benzo[d]imidazole

: 6-nitro-1-phenyl-1H-benzo[d]imidazole

Guidance literature:: With copper(l) iodide; 1,10-Phenanthroline; caesium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 48h; Inert atmosphere; Schlenk technique;
DOI:10.1002/asia.201701078