Technology Process of Benzoic acid, 2-(2-propenyl)-, methyl ester
There total 13 articles about Benzoic acid, 2-(2-propenyl)-, methyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
o-iodo-methyl-benzoic acid;
With
1-bromo-butane; iodine; magnesium;
In
tetrahydrofuran;
at -40 ℃;
for 1.75h;
Inert atmosphere;
With
copper(l) cyanide; lithium chloride;
In
tetrahydrofuran;
for 0.25h;
Inert atmosphere;
allyl bromide;
In
tetrahydrofuran;
at -40 - 20 ℃;
for 0.166667h;
Inert atmosphere;
DOI:10.1002/chem.201804131
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); lithium chloride;
In
tetrahydrofuran;
at 100 ℃;
for 12h;
Inert atmosphere;
Sealed tube;
DOI:10.1002/anie.201911372
- Guidance literature:
-
With
pyridine; nickel(II) iodide; tetrabutylammomium bromide; 4,4'-di-tert-butyl-2,2'-bipyridine; magnesium chloride; zinc;
In
N,N-dimethyl acetamide;
at 60 ℃;
for 12h;
Inert atmosphere;
DOI:10.1021/ol3013342