Silane, trimethyl[(3-methyl-2-furanyl)oxy]-

Base Information

Chemical Name:Silane, trimethyl[(3-methyl-2-furanyl)oxy]-
CAS No.:61550-03-6
Molecular Formula:C8H14O2Si
Molecular Weight:170.283
Hs Code.:
DSSTox Substance ID:DTXSID10450799
Nikkaji Number:J874.721K
Wikidata:Q82270619

Synonyms:61550-03-6;Silane, trimethyl[(3-methyl-2-furanyl)oxy]-;[(3-Methyl-2-furyl)oxy]trimethylsilane;DTXSID10450799;3-Methyl-2-(trimethylsiloxy)furan;3-methyl-2-(trimethylsilyloxy)furan;MFCD28660145;SY270728

Suppliers and Price of Silane, trimethyl[(3-methyl-2-furanyl)oxy]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AK Scientific
Silane,trimethyl[(3-methyl-2-furanyl)oxy]-
1g
$ 1396.00

Total 5 raw suppliers

Chemical Property of Silane, trimethyl[(3-methyl-2-furanyl)oxy]-

Chemical Property:

PSA：22.37000
LogP:2.80170
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:170.076306220
Heavy Atom Count:11
Complexity:131

Purity/Quality:

97% ^*data from raw suppliers

Silane,trimethyl[(3-methyl-2-furanyl)oxy]- ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(OC=C1)O[Si](C)(C)C

Technology Process of Silane, trimethyl[(3-methyl-2-furanyl)oxy]-

There total 5 articles about Silane, trimethyl[(3-methyl-2-furanyl)oxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 22122-36-7
3-methyl-5H-furan-2-one

: 27607-77-8
trimethylsilyl trifluoromethanesulfonate

: 61550-03-6
2-trimethylsilyloxy-3-methylfurane

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/ja804659n

Reference yield: 56.0%

: 75-77-4
chloro-trimethyl-silane

: 22122-36-7
3-methyl-5H-furan-2-one

: 61550-03-6
2-trimethylsilyloxy-3-methylfurane

Guidance literature:: With lithium diisopropyl amide; at -78 - 0 ℃; for 1.16667h;
DOI:10.1039/b002903n

Reference yield:

: 616-02-4
citraconic acid anhydride

: 61550-03-6
2-trimethylsilyloxy-3-methylfurane

Guidance literature:: Multi-step reaction with 2 steps

1.1: dicyclohexylamine / methanol / 3.5 h / -15 - 20 °C

1.2: ClCO₂Bu / CH₂Cl₂ / 12 h / -12 °C

1.3: NaBH₄ / tetrahydrofuran / 3 h / 0 °C

2.1: 56 percent / LDA / 1.17 h / -78 - 0 °C

With N-cyclohexyl-cyclohexanamine; lithium diisopropyl amide; In methanol;
DOI:10.1039/b002903n