1,1'-[(2-Iodophenyl)methylene]dibenzene

Base Information

Chemical Name:1,1'-[(2-Iodophenyl)methylene]dibenzene
CAS No.:61593-11-1
Molecular Formula:C19H15I
Molecular Weight:370.233
Hs Code.:
DSSTox Substance ID:DTXSID10710527
Wikidata:Q82645886

Synonyms:61593-11-1;1,1'-[(2-Iodophenyl)methylene]dibenzene;SCHEMBL16632474;DTXSID10710527

Suppliers and Price of 1,1'-[(2-Iodophenyl)methylene]dibenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1'-[(2-Iodophenyl)methylene]dibenzene

Chemical Property:

XLogP3:5.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:3
Exact Mass:370.02185
Heavy Atom Count:20
Complexity:258

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(C2=CC=CC=C2)C3=CC=CC=C3I

Technology Process of 1,1'-[(2-Iodophenyl)methylene]dibenzene

There total 7 articles about 1,1'-[(2-Iodophenyl)methylene]dibenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 717882-59-2
(2-iodophenyl)diphenylmethanol

: 61593-11-1
((2-iodophenyl)methylene)dibenzene 2-benzhydrylaniline

Guidance literature:: With iodine; hypophosphorous acid; acetic acid; In water; at 60 ℃;
DOI:10.1021/acs.orglett.7b03564

Reference yield:

: 61593-10-0
o-nitrotriphenylmethane

: 61593-11-1
((2-iodophenyl)methylene)dibenzene 2-benzhydrylaniline

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd-C / ethanol

2: (i) aq. NaNO₂, aq. HCl, (ii) aq. KI

With hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1016/0040-4020(76)85198-8

Reference yield:

: 2835-77-0
(2-aminophenyl)(phenyl)methanone

: 61593-11-1
((2-iodophenyl)methylene)dibenzene 2-benzhydrylaniline

Guidance literature:: Multi-step reaction with 3 steps

1.1: diethyl ether; tetrahydrofuran / 2 h / 20 °C

2.1: trifluoroacetic acid; triethylsilane / dichloromethane / 2 h / 20 °C

3.1: acetic acid; sulfuric acid / water / 0.25 h / 0 °C

3.2: 1 h / 20 - 60 °C

With triethylsilane; sulfuric acid; acetic acid; trifluoroacetic acid; In tetrahydrofuran; diethyl ether; dichloromethane; water;
DOI:10.1002/ejoc.201501356