1-Phenyl-5-acenaphtheneacetic acid

Base Information

Chemical Name:1-Phenyl-5-acenaphtheneacetic acid
CAS No.:71823-44-4
Molecular Formula:C₂₀H₁₆O₂
Molecular Weight:288.346
Hs Code.:
DSSTox Substance ID:DTXSID30992520
Nikkaji Number:J72.493I
ChEMBL ID:CHEMBL3251912
Mol file:71823-44-4.mol

Synonyms:1-Phenyl-5-acenaphtheneacetic acid;BRN 2149147;71823-44-4;5-Acenaphtheneacetic acid, 1-phenyl-;CHEMBL3251912;SCHEMBL11316145;DTXSID30992520;LS-7853;(1-Phenyl-1,2-dihydroacenaphthylen-5-yl)acetic acid

Suppliers and Price of 1-Phenyl-5-acenaphtheneacetic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 1-Phenyl-5-acenaphtheneacetic acid

Chemical Property:

Vapor Pressure:2.08E-10mmHg at 25°C
Boiling Point:489.8°Cat760mmHg
Flash Point:386.3°C
PSA：37.30000
Density:1.272g/cm³
LogP:4.15490
XLogP3:4.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:288.115029749
Heavy Atom Count:22
Complexity:412

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C(C2=CC=CC3=C(C=CC1=C32)CC(=O)O)C4=CC=CC=C4

Technology Process of 1-Phenyl-5-acenaphtheneacetic acid

There total 6 articles about 1-Phenyl-5-acenaphtheneacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16618-72-7
3-phenyl-1-indanone

: 71823-44-4
1-Phenyl-5-acenaphtheneacetic acid

Guidance literature:: Multi-step reaction with 6 steps

1: (i) Zn, I₂, Et₂O, (ii) H₂, Pd-C, EtOH

2: (i) LiAlH₄, THF, (ii) aq. HBr, (iii) /BRN= 3587243/, aq. acetone

3: aq. NaOH / Heating

4: (i) PCl₅, benzene, (ii) AlCl₃

5: Zn, I₂ / diethyl ether / Heating

6: (i) Pd-C, (ii) aq. NaOH

With sodium hydroxide; iodine; zinc; In diethyl ether;
DOI:10.1021/jm00198a007

Reference yield:

: 71823-49-9
3-(3-phenylindan-1-yl)propionitrile

: 71823-44-4
1-Phenyl-5-acenaphtheneacetic acid

Guidance literature:: Multi-step reaction with 4 steps

1: aq. NaOH / Heating

2: (i) PCl₅, benzene, (ii) AlCl₃

3: Zn, I₂ / diethyl ether / Heating

4: (i) Pd-C, (ii) aq. NaOH

With sodium hydroxide; iodine; zinc; In diethyl ether;
DOI:10.1021/jm00198a007

Reference yield:

: 71823-41-1
ethyl 3-phenylindan-1-acetate

: 71823-44-4
1-Phenyl-5-acenaphtheneacetic acid

Guidance literature:: Multi-step reaction with 5 steps

1: (i) LiAlH₄, THF, (ii) aq. HBr, (iii) /BRN= 3587243/, aq. acetone

2: aq. NaOH / Heating

3: (i) PCl₅, benzene, (ii) AlCl₃

4: Zn, I₂ / diethyl ether / Heating

5: (i) Pd-C, (ii) aq. NaOH

With sodium hydroxide; iodine; zinc; In diethyl ether;
DOI:10.1021/jm00198a007