2,4-Dinitrobenzyl bromide

Base Information

Chemical Name:2,4-Dinitrobenzyl bromide
CAS No.:3013-38-5
Molecular Formula:C7H5 Br N2 O4
Molecular Weight:261.032
Hs Code.:2904909090
DSSTox Substance ID:DTXSID10427320
Nikkaji Number:J1.815.040I
Wikidata:Q82239988
Mol file:3013-38-5.mol

Synonyms:2,4-DINITROBENZYL BROMIDE;3013-38-5;2,4-Dinitrobenzylbromide;1-(bromomethyl)-2,4-dinitrobenzene;2,4-DINITRO BENZYL BROMIDE;Benzene, 1-(bromomethyl)-2,4-dinitro-;2,4-Dinitrobenzylbromid;SCHEMBL136817;DTXSID10427320;AMY28027;MFCD00792410;AKOS009158628;AS-58373;FT-0634602;EN300-204726

Suppliers and Price of 2,4-Dinitrobenzyl bromide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2,4-DINITROBENZYL BROMIDE 95.00%
5MG
$ 504.37

AK Scientific
2,4-Dinitrobenzylbromide
500mg
$ 222.00

AK Scientific
2,4-Dinitrobenzylbromide
250mg
$ 171.00

AHH
2,4-Dinitrobenzylbromide 98%
50g
$ 518.00

Total 21 raw suppliers

Chemical Property of 2,4-Dinitrobenzyl bromide

Chemical Property:

Vapor Pressure:4.63E-05mmHg at 25°C
Melting Point:50-52°C
Boiling Point:360.3°Cat760mmHg
Flash Point:171.7°C
PSA：91.64000
Density:1.83g/cm³
LogP:3.44430
XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:259.94327
Heavy Atom Count:14
Complexity:237

Purity/Quality:

99%, ^*data from raw suppliers

2,4-DINITROBENZYL BROMIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Statements: 36/37/38
Safety Statements: 26-36/37/39

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C=C1[N+](=O)[O-])[N+](=O)[O-])CBr

Technology Process of 2,4-Dinitrobenzyl bromide

There total 5 articles about 2,4-Dinitrobenzyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 4836-66-2
2,4-dinitrobenzyl alcohol

: 3013-38-5
2,4-dinitrobenzyl bromide

Guidance literature:: With carbon tetrabromide; triphenylphosphine; In ethyl acetate; at 20 ℃; for 1h;
DOI:10.1021/acs.jmedchem.0c01374

Reference yield:

: 121-14-2
2,4-dinitrotoluene

: 3013-38-5
2,4-dinitrobenzyl bromide

Guidance literature:: With bromine; Explosionsgefahr bei Anwendung von erhoehtem Druck;

Reference yield:

: 610-30-0
2,4-dinitrobenzoic acid

: 3013-38-5
2,4-dinitrobenzyl bromide

Guidance literature:: Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate; sodium tetrahydroborate / tetrahydrofuran / 1 h / 0 - 20 °C

2: carbon tetrabromide; triphenylphosphine / ethyl acetate / 1 h / 20 °C

With sodium tetrahydroborate; carbon tetrabromide; boron trifluoride diethyl etherate; triphenylphosphine; In tetrahydrofuran; ethyl acetate;
DOI:10.1021/acs.jmedchem.0c01374