Furan, 2-methyl-5-(2-nitroethenyl)-, (E)-

Base Information

• Chemical Name: Furan, 2-methyl-5-(2-nitroethenyl)-, (E)-
• CAS No.: 61691-99-4
• Molecular Formula: C₇H₇NO₃
• Molecular Weight: 153.137

Synonyms:2-Methyl-5-(2-nitro-vinyl)-furan;2-Methyl-5-(2-nitrovinyl)-furan;2-Methyl-5-((E)-2-nitro-vinyl)-furan;2-methyl-5-(E-2-nitroethenyl)furan;2-methyl-5-(2-nitrovinyl)furan;

Chemical Property of Furan, 2-methyl-5-(2-nitroethenyl)-, (E)-

Chemical Property:

• PSA: 58.96000
• LogP: 2.35860

Purity/Quality:

2-Methyl-5-[(E)-2-nitrovinyl]furan ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Furan, 2-methyl-5-(2-nitroethenyl)-, (E)-

There total 4 articles about Furan, 2-methyl-5-(2-nitroethenyl)-, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Sucrose (57-50-1) → 2-(5-methyl-2-furyl)-1-nitroethylene (61691-99-4)

Guidance literature:

Multi-step reaction with 2 steps

1: aqueous H₂SO₄; tin (IV)-chloride; sodium chloride

2: aqueous KOH-solution

With potassium hydroxide; sulfuric acid; tin(IV) chloride; sodium chloride;

DOI:10.1021/ja01345a057

Reference yield:

5-Methylfurfural (620-02-0) + nitromethane (75-52-5) → 2-(5-methyl-2-furyl)-1-nitroethylene (61691-99-4)

Guidance literature:

With potassium hydroxide;

DOI:10.1021/ja01345a057

Reference yield:

→ 2-(5-methyl-2-furyl)-1-nitroethylene (61691-99-4)

Guidance literature:

5-Methylfurfurol, Nitromethan, wss.methanol.NaOH, Kuehlung;

upstream raw materials:

5-Methylfurfural

nitromethane

Sucrose

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