Technology Process of Stibonium, tetrakis(4-methylphenyl)-, bromide
There total 5 articles about Stibonium, tetrakis(4-methylphenyl)-, bromide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
toluene;
mixt. of Sb and Sn deriv. in a molar ratio 2:1 was allowed to stand in an evacuated glass ampoule at room temp. for 24 h; crystals of (p-Tol)4SbBr filtered off; filtrate evapd; residue chromd. on SiO2; identified by elem. anal. and NMR spectrum;
- Guidance literature:
-
In
toluene;
mixt. of equimolar amts. of Sb and Sn deriv. was allowed to stand in an evacuated glass ampoule at room temp. for 24 h; crystals of (p-Tol)4SbBr filtered off; filtrate evapd; residue chromd. on SiO2; identified by elem. anal.;
- Guidance literature:
-
In
toluene;
mixt. of Sb and Sn deriv. was allowed to stand in an evacuated glass ampoule at room temp. for 72 h; crystals of (p-Tol)4SbBr filtered off; filtrate evapd; residue chromd. on SiO2; identified by elem. anal. and NMR spectrum;
