Stibonium, tetrakis(4-methylphenyl)-, bromide

Base Information

Chemical Name:Stibonium, tetrakis(4-methylphenyl)-, bromide
CAS No.:61705-01-9
Molecular Formula:C28H28Sb.Br
Molecular Weight:566.184
Hs Code.:

Synonyms:

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Chemical Property of Stibonium, tetrakis(4-methylphenyl)-, bromide

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of Stibonium, tetrakis(4-methylphenyl)-, bromide

There total 5 articles about Stibonium, tetrakis(4-methylphenyl)-, bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 13328-67-1,51017-91-5
penta(p-tolyl)antimony(V)

: 996-08-7
dibutyltin dibromide

: 61705-01-9
tetra-para-tolylstiboniumbromide

: 70841-00-8
dibutyl di(p-methylphenyl)tin

Guidance literature:: In toluene; mixt. of Sb and Sn deriv. in a molar ratio 2:1 was allowed to stand in an evacuated glass ampoule at room temp. for 24 h; crystals of (p-Tol)4SbBr filtered off; filtrate evapd; residue chromd. on SiO2; identified by elem. anal. and NMR spectrum;

Reference yield: 93.0%

: 13328-67-1,51017-91-5
penta(p-tolyl)antimony(V)

: 996-08-7
dibutyltin dibromide

: 297162-92-6
dibutyl(p-tolyl)stannyl bromide

: 61705-01-9
tetra-para-tolylstiboniumbromide

Guidance literature:: In toluene; mixt. of equimolar amts. of Sb and Sn deriv. was allowed to stand in an evacuated glass ampoule at room temp. for 24 h; crystals of (p-Tol)4SbBr filtered off; filtrate evapd; residue chromd. on SiO2; identified by elem. anal.;

Reference yield: 91.0%

: 962-89-0
triphenyltin bromide

: 13328-67-1,51017-91-5
penta(p-tolyl)antimony(V)

: 15807-28-0
triphenyl(p-tolyl)tin

: 61705-01-9
tetra-para-tolylstiboniumbromide

Guidance literature:: In toluene; mixt. of Sb and Sn deriv. was allowed to stand in an evacuated glass ampoule at room temp. for 72 h; crystals of (p-Tol)4SbBr filtered off; filtrate evapd; residue chromd. on SiO2; identified by elem. anal. and NMR spectrum;