dibutyl di(p-methylphenyl)tin

Base Information

Chemical Name:dibutyl di(p-methylphenyl)tin
CAS No.:70841-00-8
Molecular Formula:C₂₂H₃₂Sn
Molecular Weight:415.206
Hs Code.:

Synonyms:dibutyl di(p-methylphenyl)tin

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Chemical Property of dibutyl di(p-methylphenyl)tin

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Technology Process of dibutyl di(p-methylphenyl)tin

There total 4 articles about dibutyl di(p-methylphenyl)tin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 13328-67-1,51017-91-5
penta(p-tolyl)antimony(V)

: 996-08-7
dibutyltin dibromide

: 61705-01-9
tetra-para-tolylstiboniumbromide

: 70841-00-8
dibutyl di(p-methylphenyl)tin

Guidance literature:: In toluene; mixt. of Sb and Sn deriv. in a molar ratio 2:1 was allowed to stand in an evacuated glass ampoule at room temp. for 24 h; crystals of (p-Tol)4SbBr filtered off; filtrate evapd; residue chromd. on SiO2; identified by elem. anal. and NMR spectrum;

Reference yield: 92.0%

: 683-18-1
dibutyltin chloride

: 4294-57-9
para-methylphenylmagnesium bromide

: 70841-00-8
dibutyl di(p-methylphenyl)tin

Guidance literature:: In diethyl ether; Sn compd. was added to soln. of Mg compd. in Et2O; stirred at room temp.for 24 h; H2O added; aq. layer extd. (Et2O); combined org. phase washed (satd. aq.soln. of NH4Cl); dried (MgSO4); filtered; concd. (vac.);
DOI:10.1021/om900326g

Reference yield: 81.0%

: 624-31-7
4-tolyl iodide

: 683-18-1
dibutyltin chloride

: 70841-00-8
dibutyl di(p-methylphenyl)tin

Guidance literature:: dibutyltin chloride; With naphthalene; lithium; In tetrahydrofuran; at 20 ℃; for 3h; Inert atmosphere;

4-tolyl iodide; In tetrahydrofuran; at 0 - 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/jacs.5b06587