Technology Process of 2H-Purin-2-one, 1,7-dihydro-6-[(phenylmethyl)amino]-, hydrazone
There total 6 articles about 2H-Purin-2-one, 1,7-dihydro-6-[(phenylmethyl)amino]-, hydrazone which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: water / 4.5 h / 70 °C
2: water; sodium hydroxide / 3 h / 20 °C
3: hydrogenchloride; zinc(II) chloride; sodium nitrite / water / 1 h / -5 - 5 °C
4: isopropyl alcohol / 3.5 h / 82 °C
5: hydrazine hydrate / water / 1.5 h / Reflux
With
hydrogenchloride; water; hydrazine hydrate; sodium hydroxide; zinc(II) chloride; sodium nitrite;
In
water; isopropyl alcohol;
DOI:10.1080/15257770.2011.602655
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrogenchloride; zinc(II) chloride; sodium nitrite / water / 1 h / -5 - 5 °C
2: isopropyl alcohol / 3.5 h / 82 °C
3: hydrazine hydrate / water / 1.5 h / Reflux
With
hydrogenchloride; hydrazine hydrate; zinc(II) chloride; sodium nitrite;
In
water; isopropyl alcohol;
DOI:10.1080/15257770.2011.602655
