Technology Process of Methylene-2-azido-6-benzylaminopurine
There total 8 articles about Methylene-2-azido-6-benzylaminopurine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogenchloride; acetic acid; sodium nitrite;
In
water;
at 20 ℃;
for 96h;
Darkness;
DOI:10.1080/15257770.2011.602655
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrazine hydrate / water / 1.5 h / Reflux
2: hydrogenchloride; acetic acid; sodium nitrite / water / 96 h / 20 °C / Darkness
With
hydrogenchloride; hydrazine hydrate; acetic acid; sodium nitrite;
In
water;
DOI:10.1080/15257770.2011.602655
- Guidance literature:
-
Multi-step reaction with 6 steps
1: water / 4.5 h / 70 °C
2: water; sodium hydroxide / 3 h / 20 °C
3: hydrogenchloride; zinc(II) chloride; sodium nitrite / water / 1 h / -5 - 5 °C
4: isopropyl alcohol / 3.5 h / 82 °C
5: hydrazine hydrate / water / 1.5 h / Reflux
6: hydrogenchloride; acetic acid; sodium nitrite / water / 96 h / 20 °C / Darkness
With
hydrogenchloride; water; hydrazine hydrate; acetic acid; sodium hydroxide; zinc(II) chloride; sodium nitrite;
In
water; isopropyl alcohol;
DOI:10.1080/15257770.2011.602655