Germane, [2-[4-(2-ethoxyethoxy)phenyl]ethyl](4-methoxyphenyl)dimethyl-

Base Information

Chemical Name:Germane, [2-[4-(2-ethoxyethoxy)phenyl]ethyl](4-methoxyphenyl)dimethyl-
CAS No.:618887-49-3
Molecular Formula:C21H30GeO3
Molecular Weight:403.057
Hs Code.:

Synonyms:

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Chemical Property of Germane, [2-[4-(2-ethoxyethoxy)phenyl]ethyl](4-methoxyphenyl)dimethyl-

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of Germane, [2-[4-(2-ethoxyethoxy)phenyl]ethyl](4-methoxyphenyl)dimethyl-

There total 1 articles about Germane, [2-[4-(2-ethoxyethoxy)phenyl]ethyl](4-methoxyphenyl)dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 628-34-2
2-chloroethyl ethyl ether

: 618887-48-2
4-(2-[(4-methoxyphenyl)dimethylgermanyl]ethyl)phenol

: 618887-49-3
(2-[4-(2-ethoxyethoxy)phenyl]ethyl)-(4-methoxyphenyl)dimethylgermane

Guidance literature:: With caesium carbonate; In acetonitrile; (N2); addn. of ether deriv., tetrabutylammonium iodide and cesium carbonate to soln. of germanium compd. in acetonitrile, refluxing at 85°C for 17 h; cooling, filtration, evapn., chromy. (petroleum ether/ethyl acetate (20:1)), MAS;
DOI:10.1039/b703022c

Reference yield: 67.0%

: 618887-49-3
(2-[4-(2-ethoxyethoxy)phenyl]ethyl)-(4-methoxyphenyl)dimethylgermane

: 75-36-5
acetyl chloride

: 100-06-1
1-(4-methoxyphenyl)ethanone

Guidance literature:: acetyl chloride; With aluminium trichloride; In dichloromethane; at -78 ℃;

(2-[4-(2-ethoxyethoxy)phenyl]ethyl)-(4-methoxyphenyl)dimethylgermane; In dichloromethane; at -78 - 20 ℃; for 3h;
DOI:10.1055/s-2005-872258

Reference yield: 60.0%

: 618887-49-3
(2-[4-(2-ethoxyethoxy)phenyl]ethyl)-(4-methoxyphenyl)dimethylgermane

: 7647-01-0,15364-23-5
hydrogenchloride

: 1693-86-3
3-hexylthiophene

: 438587-18-9
{2-[4-(2-ethoxyethoxy)phenyl]ethyl}-(4-hexylthiophen-2-yl)dimethylgermane

Guidance literature:: With LiN(CH(CH₃)2)2; In tetrahydrofuran; diethyl ether; hexane; (N2); addn. of 1 M ethereal HCl to germanium compd., stirring for 16 h, evapn.; addn. of amide deriv. in hexane, THF and ethylbenzene (6:5:3) tothiophene deriv. in THF, stirring for 40 min at -40°C, addn. to cold soln. of obtained oil in THF; stirring for 1 h at -40°C, warming to room temp., stirring for 1 h, addn. of saturd. aqueous NH4Cl, extn. (ether), drying with MgSO4, evapn., chromy. (petroleum ether/ethyl acetate (9:1)), MAS;
DOI:10.1039/b703022c