Pentaborane(9), 1-methyl-

Base Information

Chemical Name:Pentaborane(9), 1-methyl-
CAS No.:19495-55-7
Molecular Formula:CH₁₁B₅
Molecular Weight:77.1533
Hs Code.:

Synonyms:

Suppliers and Price of Pentaborane(9), 1-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Pentaborane(9), 1-methyl-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Pentaborane(9), 1-methyl-

There total 1 articles about Pentaborane(9), 1-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 23753-67-5
1-bromopentaborane⁽⁹⁾

: 19624-22-7
pentaborane⁽⁹⁾

: 19495-55-7
1-CH₃B₅H₈

: 121-43-7,63156-11-6
Trimethyl borate

: 23753-64-2
2-bromo-pentaborane⁽⁹⁾

Guidance literature:: With (CH₃)2O; In Dimethyl ether; byproducts: H2, CH3Br; at 24°C, 48h;;
DOI:10.1021/ja01094a055

Reference yield: 88.5%

: 18283-93-7
tetraborane

: 19495-55-7
1-CH₃B₅H₈

: 93110-36-2
1:2'-[B₄H₉][1'-CH₃B₅H₇]

: 1333-74-0
hydrogen

Guidance literature:: platinum(II) bromde; In neat (no solvent); PtBr2, B4H10, and 1-MeB5H8 stirred in vac. at room temp. for 4 h, (i), -196°C fraction recondensed over PtBr2 and stirred at room temp. for addnl. 12 h with H2 and product removal every 4 h as in (i); (i) fractionated through -50, -196°C trap series, -50°C fraction purified on low-temp. distn. column (exit temp. of -40 to -42°C);
DOI:10.1021/ja00337a024