(-)-[(2-methylbutoxy)methyl]benzene

Base Information

Chemical Name:(-)-[(2-methylbutoxy)methyl]benzene
CAS No.:32793-87-6
Molecular Formula:C12H18 O
Molecular Weight:178.274
Hs Code.:2909309090
Mol file:32793-87-6.mol

Synonyms:Benzene,[(2-methylbutoxy)methyl]-, (R)-; Ether, benzyl 2-methylbutyl, (-)- (8CI)

Suppliers and Price of (-)-[(2-methylbutoxy)methyl]benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 5 raw suppliers

Chemical Property of (-)-[(2-methylbutoxy)methyl]benzene

Chemical Property:

Boiling Point:230.1°Cat760mmHg
Flash Point:93.7°C
PSA：9.23000
Density:0.914g/cm³
LogP:3.24930

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (-)-[(2-methylbutoxy)methyl]benzene

There total 5 articles about (-)-[(2-methylbutoxy)methyl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 63930-49-4
(R)-3-(benzyloxy)-2-methylpropan-1-ol

: 32793-87-6
(R)-1-<(2-methylbutoxy)methyl>benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / Ph₃P, N-bromosuccinimide / CH₂Cl₂ / 23 h / Ambient temperature

2: CuCN / 1.) THF, Et₂O, 0 deg C, 5 min, 2.) THF, -20 deg C, 4 h; r.t., overnight

With N-Bromosuccinimide; triphenylphosphine; In dichloromethane;
DOI:10.1021/jo00091a022

Reference yield:

: 81927-55-1
O-benzyl 2,2,2-trichloroacetimidate

: 32793-87-6
(R)-1-<(2-methylbutoxy)methyl>benzene

Guidance literature:: Multi-step reaction with 4 steps

1: 83 percent / trifluoromethanesulfonic acid / cyclohexane; CH₂Cl₂ / 24 h

2: 98 percent / LiAlH₄ / diethyl ether / 1.) O deg C to r.t., 2.) r.t., 30 min

3: 86 percent / Ph₃P, N-bromosuccinimide / CH₂Cl₂ / 23 h / Ambient temperature

4: CuCN / 1.) THF, Et₂O, 0 deg C, 5 min, 2.) THF, -20 deg C, 4 h; r.t., overnight

With N-Bromosuccinimide; lithium aluminium tetrahydride; trifluorormethanesulfonic acid; triphenylphosphine; In diethyl ether; dichloromethane; cyclohexane;
DOI:10.1021/jo00091a022

Reference yield:

: 74924-27-9
methyl (S)-3-benzyloxy-2-methylpropanoate

: 32793-87-6
(R)-1-<(2-methylbutoxy)methyl>benzene

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / LiAlH₄ / diethyl ether / 1.) O deg C to r.t., 2.) r.t., 30 min

2: 86 percent / Ph₃P, N-bromosuccinimide / CH₂Cl₂ / 23 h / Ambient temperature

3: CuCN / 1.) THF, Et₂O, 0 deg C, 5 min, 2.) THF, -20 deg C, 4 h; r.t., overnight

With N-Bromosuccinimide; lithium aluminium tetrahydride; triphenylphosphine; In diethyl ether; dichloromethane;
DOI:10.1021/jo00091a022