7-Chloro-1H-1,5-benzodiazepine-2,4(3H,5H)-dione

Base Information

Chemical Name:7-Chloro-1H-1,5-benzodiazepine-2,4(3H,5H)-dione
CAS No.:61911-86-2
Molecular Formula:C9H7ClN2O2
Molecular Weight:210.62
Hs Code.:
DSSTox Substance ID:DTXSID30438913
Nikkaji Number:J999.227H
Wikidata:Q82254757
ChEMBL ID:CHEMBL1642300

Synonyms:7-Chloro-1H-1,5-benzodiazepine-2,4(3H,5H)-dione;61911-86-2;CHEMBL1642300;DTXSID30438913;AKOS020298956

Suppliers and Price of 7-Chloro-1H-1,5-benzodiazepine-2,4(3H,5H)-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-Chloro-1H-1,5-benzodiazepine-2,4(3H,5H)-dione

Chemical Property:

XLogP3:0.8
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:210.0196052
Heavy Atom Count:14
Complexity:270

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C(=O)NC2=C(C=C(C=C2)Cl)NC1=O

Technology Process of 7-Chloro-1H-1,5-benzodiazepine-2,4(3H,5H)-dione

There total 1 articles about 7-Chloro-1H-1,5-benzodiazepine-2,4(3H,5H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7-chloro-3-((dimethylamino)methylene)-1H-benzo[b][1,4]diazepine-2,4(3H,5H)-dione

: 2582-30-1
aminoguanidine bicarbonate

: 61-82-5
3-amino-1,2,4-triazole

: 61911-86-2
7-chloro-1H-1,5-benzodiazepine-2,4(3H,5H)-dione

Guidance literature:: With sodium ethanolate; In ethanol;
DOI:10.1016/j.tet.2017.03.079

Reference yield:

: 603-33-8
triphenylbismuthane

: 61911-86-2
7-chloro-1H-1,5-benzodiazepine-2,4(3H,5H)-dione

: 22316-55-8
N-desmethylclobazam

Guidance literature:: With copper diacetate; In dichloromethane;
DOI:10.1016/j.bmcl.2010.10.131

Reference yield:

: 61911-86-2
7-chloro-1H-1,5-benzodiazepine-2,4(3H,5H)-dione

: 36985-18-9
8-chloro-3-(dimethylamino-methylene)-1-phenyl-1,5-dihydro-benzo[b][1,4]diazepine-2,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: copper diacetate / dichloromethane

2: 140 °C

With copper diacetate; In dichloromethane;
DOI:10.1016/j.bmcl.2010.10.131