2-Oxo-1,2-diphenylethyl dihydrogen phosphate

Base Information

• Chemical Name: 2-Oxo-1,2-diphenylethyl dihydrogen phosphate
• CAS No.: 7509-04-8
• Molecular Formula: C14H13O5P
• Molecular Weight: 292.2238
• NSC Number: 407202
• DSSTox Substance ID: DTXSID40331300
• Nikkaji Number: J496.610D
• Mol file: 7509-04-8.mol

Synonyms:7509-04-8;NSC407202;SCHEMBL7720549;DTXSID40331300;NSC-407202;2-Oxo-1,2-diphenylethyl dihydrogen phosphate

Chemical Property of 2-Oxo-1,2-diphenylethyl dihydrogen phosphate

Chemical Property:

• Vapor Pressure: 2.13E-11mmHg at 25°C
• Boiling Point: 514.2°Cat760mmHg
• Flash Point: 264.8°C
• Density: 1.405g/cm³
• XLogP3: 1.6
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 5
• Exact Mass: 292.05006051
• Heavy Atom Count: 20
• Complexity: 366

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C(C(=O)C2=CC=CC=C2)OP(=O)(O)O

Technology Process of 2-Oxo-1,2-diphenylethyl dihydrogen phosphate

There total 10 articles about 2-Oxo-1,2-diphenylethyl dihydrogen phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

2-hydroxy-2-phenylacetophenone (119-53-9,579-44-2) + Methylpyridinium dichlorophosphate → 2-Oxo-1,2-diphenylethyl dihydrogen phosphate (7509-04-8)

Guidance literature:

With pyridine; for 6h; Heating;

DOI:10.1016/S0040-4020(01)87875-3

Reference yield: 19.0%

methanol (67-56-1) + Bis(2-cyanoethyl) 2-oxo-1,2-diphenylethyl phosphate (144758-78-1) → benzoin dimethyl ketal (1889-85-6) + 2-Oxo-1,2-diphenylethyl dihydrogen phosphate (7509-04-8) + Methyl 2-oxo-1,2-diphenylethyl hydrogen phosphate

Guidance literature:

With sodium hydroxide; at 50 ℃; for 0.75h;

Reference yield:

2-chloro-4,5-diphenyl-2-oxo-1,3,2λ5-dioxaphosphole (149725-58-6) → 2-Oxo-1,2-diphenylethyl dihydrogen phosphate (7509-04-8)

Guidance literature:

With water; In tetrahydrofuran; for 0.5h;

upstream raw materials:

methanol

Bis(2-cyanoethyl) 2-oxo-1,2-diphenylethyl phosphate

2-hydroxy-2-phenylacetophenone

Phosphoric acid mono-[phenyl-(2-phenyl-[1,3]dioxolan-2-yl)-methyl] ester

Downstream raw materials:

2-phenylbenzofuran