[(4-methylphenyl)sulfonyl](phenylsulfanyl)methanethione

Base Information

• Chemical Name: [(4-methylphenyl)sulfonyl](phenylsulfanyl)methanethione
• CAS No.: 31536-16-0
• Molecular Formula: C14H12 O2 S3
• Molecular Weight: 308.4389

Synonyms:Carbonicacid, trithio-, phenyl p-tolyl ester, thiolo',thiolo'-dioxide (8CI);Methane(dithioic) acid, [(4-methylphenyl)sulfonyl]-, phenyl ester (9CI); NSC277532

Chemical Property of [(4-methylphenyl)sulfonyl](phenylsulfanyl)methanethione

Chemical Property:

• Vapor Pressure: 2.61E-08mmHg at 25°C
• Boiling Point: 463°Cat760mmHg
• Flash Point: 233.8°C
• Density: 1.39g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of [(4-methylphenyl)sulfonyl](phenylsulfanyl)methanethione

There total 2 articles about [(4-methylphenyl)sulfonyl](phenylsulfanyl)methanethione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenyl chlorodithioformate (16911-89-0) + sodium 4-methylbenzenesulfinate (824-79-3) → phenyl C-(4-methylphenylsulfonyl)dithiophormate (31536-16-0)

Guidance literature:

In N,N-dimethyl-formamide;

Reference yield:

→ phenyl C-(4-methylphenylsulfonyl)dithiophormate (31536-16-0)

Guidance literature:

p-CH3-C6H4-SO2^-, Cl-CS-S-C6H5;

DOI:10.1039/C29710000314

Reference yield: 94.0%

9-methylanthracene (779-02-2) + phenyl C-(4-methylphenylsulfonyl)dithiophormate (31536-16-0) → (+/-)-9,10-dihydro-10-methyl-12-(4-methylphenylsulfonyl)-12-(phenylthio)-10,9-(epithiomethano)anthracene

Guidance literature:

In chloroform; at 20 ℃; for 4h;

DOI:10.1002/hc.10119

upstream raw materials:

phenyl chlorodithioformate

sodium 4-methylbenzenesulfinate

Downstream raw materials:

2-Methyl-2-phenylsulfanylthiocarbonyl-malonic acid diethyl ester

1.1.2-Tris(phenylthio)-2-p-tolylsulfonylaethylen

Trithiocarbonic acid phenyl ester phenylsulfanyl-(toluene-4-sulfonyl)-methyl ester

5-phenylsulfanyl-5-(toluene-4-sulfonyl)-3-(2,4,6-trimethyl-phenyl)-[1,4,2]oxathiazole

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