2-Cyclododecen-1-ol, (E)-

Base Information

• Chemical Name: 2-Cyclododecen-1-ol, (E)-
• CAS No.: 6221-49-4
• Molecular Formula: C₁₂H₂₂O
• Molecular Weight: 182.306
• Mol file: 6221-49-4.mol

Synonyms:

Chemical Property of 2-Cyclododecen-1-ol, (E)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Cyclododecen-1-ol, (E)-

There total 1 articles about 2-Cyclododecen-1-ol, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2-epoxycyclododecane (286-99-7) → (E)-2-cyclododecen-1-ol (6221-49-4,211935-46-5) + cis,trans-1,3-cyclododecadiene (1129-92-6) + cyclododecanone (830-13-7)

Guidance literature:

With silica gel; titanium(IV) oxide; In toluene; at 108 ℃; for 1.5h; Product distribution; other catalysts, var. time;

DOI:10.1246/bcsj.67.2351

Reference yield: 87.0%

(E)-2-cyclododecen-1-ol (6221-49-4,211935-46-5) → cyclododecanone (830-13-7)

Guidance literature:

With indenylbis(triphenylphosphine)ruthenium chloride; triethylammonium hexafluorophosphate; In 1,4-dioxane; at 100 ℃; for 2.5h;

DOI:10.1021/ja00058a059

Reference yield:

(E)-2-cyclododecen-1-ol (6221-49-4,211935-46-5) + benzoyl chloride (98-88-4) → C19H26O2

Guidance literature:

With N,N,N,N,-tetramethylethylenediamine; In diethyl ether; dichloromethane; at 22 ℃; for 1h; Glovebox;

DOI:10.1021/jacs.9b04993

upstream raw materials:

1,2-epoxycyclododecane

Downstream raw materials:

cyclododecanone

Bicyclo<10.1.0>tridecan-2-ol