Phenol, 4-[[4-(2-hydroxyethoxy)phenyl]azo]-

Base Information

Chemical Name:Phenol, 4-[[4-(2-hydroxyethoxy)phenyl]azo]-
CAS No.:62257-21-0
Molecular Formula:C14H14N2O3
Molecular Weight:258.277
Hs Code.:

Synonyms:

Suppliers and Price of Phenol, 4-[[4-(2-hydroxyethoxy)phenyl]azo]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Phenol, 4-[[4-(2-hydroxyethoxy)phenyl]azo]-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Phenol, 4-[[4-(2-hydroxyethoxy)phenyl]azo]-

There total 3 articles about Phenol, 4-[[4-(2-hydroxyethoxy)phenyl]azo]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.2%

: 6421-88-1
2-(4-aminophenoxy)ethanol

: 108-95-2,27073-41-2
phenol

: 62257-21-0
4-hydroxy-4'-(2-hydroxyethoxy)azobenzene

Guidance literature:: 2-(4-aminophenoxy)ethanol; With hydrogenchloride; sodium nitrite; In water; at 0 ℃; for 1h;

phenol; With sodium hydroxide; In water; at 0 ℃; for 4h;
DOI:10.1016/j.polymer.2014.02.021

Reference yield:

: 16365-27-8
2-(4-nitrophenoxy)ethanol

: 62257-21-0
4-hydroxy-4'-(2-hydroxyethoxy)azobenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: tin(II) chloride dihdyrate / ethanol / 24 h / Reflux; Inert atmosphere

2.1: sodium nitrite; hydrogenchloride / water / 1 h / 0 °C

2.2: 4 h / 0 °C

With hydrogenchloride; tin(II) chloride dihdyrate; sodium nitrite; In ethanol; water;
DOI:10.1016/j.polymer.2014.02.021

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 62257-21-0
4-hydroxy-4'-(2-hydroxyethoxy)azobenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 6 h / 80 °C / Inert atmosphere

1.2: 24 h / 50 °C / Inert atmosphere

2.1: tin(II) chloride dihdyrate / ethanol / 24 h / Reflux; Inert atmosphere

3.1: sodium nitrite; hydrogenchloride / water / 1 h / 0 °C

3.2: 4 h / 0 °C

With hydrogenchloride; tin(II) chloride dihdyrate; potassium carbonate; sodium nitrite; In ethanol; water; N,N-dimethyl-formamide; 1.2: |Williamson Ether Synthesis;
DOI:10.1016/j.polymer.2014.02.021