[(3-Benzylpenta-1,4-dien-3-yl)oxy](triethyl)silane

Base Information

Chemical Name:[(3-Benzylpenta-1,4-dien-3-yl)oxy](triethyl)silane
CAS No.:62418-75-1
Molecular Formula:C₁₈H₂₈OSi
Molecular Weight:288.505
Hs Code.:
DSSTox Substance ID:DTXSID10508845
Wikidata:Q82366034

Synonyms:62418-75-1;[(3-Benzylpenta-1,4-dien-3-yl)oxy](triethyl)silane;DTXSID10508845

Suppliers and Price of [(3-Benzylpenta-1,4-dien-3-yl)oxy](triethyl)silane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of [(3-Benzylpenta-1,4-dien-3-yl)oxy](triethyl)silane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:9
Exact Mass:288.190942047
Heavy Atom Count:20
Complexity:284

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC[Si](CC)(CC)OC(CC1=CC=CC=C1)(C=C)C=C

Technology Process of [(3-Benzylpenta-1,4-dien-3-yl)oxy](triethyl)silane

There total 5 articles about [(3-Benzylpenta-1,4-dien-3-yl)oxy](triethyl)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 62418-65-9
Triethyl<(1,4-pentadien-3-yl)oxy>silan

: 100-44-7
benzyl chloride

: 80378-73-0
(Z)-6-phenyl-3-triethylsilyloxy-1,3-hexadiene

: 62418-75-1
3-benzyl-3-triethylsilyloxy-1,4-pentadiene

Guidance literature:: With sec.-butyllithium; In tetrahydrofuran; cyclohexane; at -78 ℃; Yield given. Yields of byproduct given;
DOI:10.1002/hlca.19810640705

Reference yield:

: 922-65-6
divinylcarbinol

: 62418-75-1
3-benzyl-3-triethylsilyloxy-1,4-pentadiene

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / imidazole / dimethylformamide / 15 h / 25 °C

2: 1.) sec-BuLi; 2.) KF / 1.) THF/cyclohexane, -78 deg C; 2.) from 0 deg C to 15 deg C, 15 h

With 1H-imidazole; potassium fluoride; sec.-butyllithium; In N,N-dimethyl-formamide;
DOI:10.1002/hlca.19810640705

Reference yield:

: 994-30-9
triethylsilyl chloride

: 62418-75-1
3-benzyl-3-triethylsilyloxy-1,4-pentadiene

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / imidazole / dimethylformamide / 15 h / 25 °C

2: 1.) sec-BuLi; 2.) KF / 1.) THF/cyclohexane, -78 deg C; 2.) from 0 deg C to 15 deg C, 15 h

With 1H-imidazole; potassium fluoride; sec.-butyllithium; In N,N-dimethyl-formamide;
DOI:10.1002/hlca.19810640705