Methanone, (2-hydroxy-4-methoxyphenyl)(3,4,5-trimethoxyphenyl)-

Base Information

Chemical Name:Methanone, (2-hydroxy-4-methoxyphenyl)(3,4,5-trimethoxyphenyl)-
CAS No.:62495-39-0
Molecular Formula:C17H18O6
Molecular Weight:318.32100
Hs Code.:

Synonyms:2-Hydroxy-3',4,4',5'-tetramethoxybenzophenon;3,4,4',5'-tetramethoxy-2'-hydroxybenzophenone;

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methanone, (2-hydroxy-4-methoxyphenyl)(3,4,5-trimethoxyphenyl)-

Chemical Property:

Melting Point:106–107°C
PSA：74.22000
LogP:2.65760

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Methanone, (2-hydroxy-4-methoxyphenyl)(3,4,5-trimethoxyphenyl)-

There total 5 articles about Methanone, (2-hydroxy-4-methoxyphenyl)(3,4,5-trimethoxyphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1027525-99-0
[2-(tert-butyl-dimethyl-silanyloxy)-4-methoxy-phenyl]-(3,4,5-trimethoxy-phenyl)-methanone

: 62495-39-0
3,4,4',5'-tetramethoxy-2'-hydroxybenzophenone

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 25 ℃; for 1h;
DOI:10.1021/jm010365+

Reference yield:

: 2675-79-8
1-bromo-3,4,5-trimethoxybenzene

: 62495-39-0
3,4,4',5'-tetramethoxy-2'-hydroxybenzophenone

Guidance literature:: Multi-step reaction with 3 steps

1.1: Mg / tetrahydrofuran / 1 h / 25 °C

1.2: tetrahydrofuran / 0.33 h / 25 °C

2.1: pyridinium dichromate / CH₂Cl₂ / 8 h / 25 °C

3.1: Bu₄NF / tetrahydrofuran / 1 h / 25 °C

With dipyridinium dichromate; tetrabutyl ammonium fluoride; magnesium; In tetrahydrofuran; dichloromethane; 1.2: Grignard reaction;
DOI:10.1021/jm010365+

Reference yield:

: [2-(tert-butyl-dimethyl-silanyloxy)-4-methoxy-phenyl]-(3,4,5-trimethoxy-phenyl)-methanol

: 62495-39-0
3,4,4',5'-tetramethoxy-2'-hydroxybenzophenone

Guidance literature:: Multi-step reaction with 2 steps

1: pyridinium dichromate / CH₂Cl₂ / 8 h / 25 °C

2: Bu₄NF / tetrahydrofuran / 1 h / 25 °C

With dipyridinium dichromate; tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm010365+