METHYL 2,3,4,6-TETRA-O-ACETYL-BETA-D-GLUCOPYRANOSIDE

Base Information

Chemical Name:METHYL 2,3,4,6-TETRA-O-ACETYL-BETA-D-GLUCOPYRANOSIDE
CAS No.:4860-85-9
Molecular Formula:C15H22 O10
Molecular Weight:362.334
Hs Code.:
Mol file:4860-85-9.mol

Synonyms:Glucopyranoside,methyl, tetraacetate, b-D- (8CI); b-D-Glucopyranoside,methyl, tetraacetate (9CI); Methyl 2,3,4,6-tetra-O-acetyl-b-D-glucopyranoside; Methyl b-D-glucopyranoside tetraacetate;NSC 48281

Suppliers and Price of METHYL 2,3,4,6-TETRA-O-ACETYL-BETA-D-GLUCOPYRANOSIDE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Usbiological
Methyl 2,3,4,6-tetra-O-acetyl-b-D-glucopyranose
2g
$ 814.00

Biosynth Carbosynth
Methyl 2,3,4,6-tetra-O-acetyl-b-D-glucopyranose
50 g
$ 2250.00

Biosynth Carbosynth
Methyl 2,3,4,6-tetra-O-acetyl-b-D-glucopyranose
25 g
$ 1560.00

Biosynth Carbosynth
Methyl 2,3,4,6-tetra-O-acetyl-b-D-glucopyranose
10 g
$ 975.00

Biosynth Carbosynth
Methyl 2,3,4,6-tetra-O-acetyl-b-D-glucopyranose
5 g
$ 650.00

Biosynth Carbosynth
Methyl 2,3,4,6-tetra-O-acetyl-b-D-glucopyranose
2 g
$ 400.00

Total 17 raw suppliers

Chemical Property of METHYL 2,3,4,6-TETRA-O-ACETYL-BETA-D-GLUCOPYRANOSIDE

Chemical Property:

Boiling Point:407.3ºC at 760 mmHg
Flash Point:176.1ºC
PSA：123.66000
Density:1.27 g/cm³
LogP:-0.28410
Storage Temp.:2-8°C

Purity/Quality:

99%, ^*data from raw suppliers

Methyl 2,3,4,6-tetra-O-acetyl-b-D-glucopyranose ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of METHYL 2,3,4,6-TETRA-O-ACETYL-BETA-D-GLUCOPYRANOSIDE

There total 83 articles about METHYL 2,3,4,6-TETRA-O-ACETYL-BETA-D-GLUCOPYRANOSIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 67-56-1
methanol

: 28244-94-2,28244-99-7,86782-41-4,131488-65-8
p-tolyl-2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranoside

: 64727-27-1
3,4,6-tri-O-acetyl-1,2-O-[1-(exo-methoxy)ethylidene]-alpha-D-glucopyranose

: 4860-85-9
methyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

: 604-70-6
Acetic acid (2R,3R,4S,5R,6S)-3,5-diacetoxy-2-acetoxymethyl-6-methoxy-tetrahydro-pyran-4-yl ester

Guidance literature:: With 3 A molecular sieve; In acetonitrile; Yields of byproduct given; electrochemical synthesis: one compartment, three-electrode, air-tight cell, vitrous carbon anode and Pt catode, 0.2 M LiBF₄ as supporting electrolyte, constant potential 1.45 V (vs standard calomel reference electrode);

Reference yield:

: 67-56-1
methanol

: 3947-62-4,6207-76-7,19235-21-3,22554-70-7,22860-22-6,47339-09-3,57884-82-9,62057-79-8,70191-05-8,109525-54-4,140147-37-1,10343-06-3
2,3,4,5-tetra-O-acetyl-D-glucopyranose

: 4860-85-9
methyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

: 604-70-6
Acetic acid (2R,3R,4S,5R,6S)-3,5-diacetoxy-2-acetoxymethyl-6-methoxy-tetrahydro-pyran-4-yl ester

Guidance literature:: With diphenylammonium trifluoromethanesulfonate; In 1,2-dichloro-ethane; toluene; at 80 ℃; for 0.5h; Overall yield = 58 percent; Overall yield = 42.1 mg; Microwave irradiation;
DOI:10.3390/molecules25051103

Reference yield:

: 67-56-1
methanol

: 604-69-3
β-D-glucose pentaacetate

: 4860-85-9
methyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside

: 604-70-6
Acetic acid (2R,3R,4S,5R,6S)-3,5-diacetoxy-2-acetoxymethyl-6-methoxy-tetrahydro-pyran-4-yl ester

Guidance literature:: With scandium tris(trifluoromethanesulfonate); In toluene; at 80 ℃; for 0.0166667h; optical yield given as %de;
DOI:10.1016/j.carres.2012.01.008