N,N'-(4-Chloro-1,3-phenylene)diacetamide

Base Information

Chemical Name:N,N'-(4-Chloro-1,3-phenylene)diacetamide
CAS No.:62595-00-0
Molecular Formula:C10H11ClN2O2
Molecular Weight:226.663
Hs Code.:
DSSTox Substance ID:DTXSID60490261
Wikidata:Q82333955

Synonyms:62595-00-0;N,N'-(4-Chloro-1,3-phenylene)diacetamide;SCHEMBL3791892;DTXSID60490261

Suppliers and Price of N,N'-(4-Chloro-1,3-phenylene)diacetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-(4-Chloro-1,3-phenylene)diacetamide

Chemical Property:

XLogP3:0.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:226.0509053
Heavy Atom Count:15
Complexity:258

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)NC1=CC(=C(C=C1)Cl)NC(=O)C

Technology Process of N,N'-(4-Chloro-1,3-phenylene)diacetamide

There total 5 articles about N,N'-(4-Chloro-1,3-phenylene)diacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 108-24-7
acetic anhydride

: 97-00-7
1-chloro-2,4-dinitro-benzene

: 5131-60-2
4-chloro-1,3-phenylenediamine

: 51867-83-5
1-amino-3-acetylamino-6-chloro-benzene

: 62595-00-0
N-(3-acetylamino-4-chlorophenyl)-acetamide

Guidance literature:: With samarium; acetic acid; In methanol; at 20 ℃; for 10h;

Reference yield: 73.0%

: 75-36-5
acetyl chloride

: 97-00-7
1-chloro-2,4-dinitro-benzene

: 62595-00-0
N-(3-acetylamino-4-chlorophenyl)-acetamide

Guidance literature:: With Low-valent Titanium reagent; In tetrahydrofuran; Ambient temperature;

Reference yield:

: 97-00-7
1-chloro-2,4-dinitro-benzene

: 62595-00-0
N-(3-acetylamino-4-chlorophenyl)-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: iron; hydrochloric acid

With hydrogenchloride; iron;
DOI:10.1002/(SICI)1520-6807(200003)37:2<183::AID-PITS9>3.0.CO;2-5