(2E)-2-(HYDROXYIMINO)-N-(3-NITROPHENYL)ACETAMIDE

Base Information

• Chemical Name: (2E)-2-(HYDROXYIMINO)-N-(3-NITROPHENYL)ACETAMIDE
• CAS No.: 17122-61-1
• Molecular Formula: C8H7 N3 O4
• Molecular Weight: 209.161
• Hs Code.: 2928000090
• Mol file: 17122-61-1.mol

Synonyms:Glyoxylanilide, 3'-nitro-, 2-oxime (8CI); Glyoxylanilide, 3'-nitro-, oxime(6CI)

Chemical Property of (2E)-2-(HYDROXYIMINO)-N-(3-NITROPHENYL)ACETAMIDE

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 111.00000
• Density: 1.47g/cm³
• LogP: 2.16600

Purity/Quality:

98% ^*data from raw suppliers

(2E)-2-(HYDROXYIMINO)-N-(3-NITROPHENYL)ACETAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (2E)-2-(HYDROXYIMINO)-N-(3-NITROPHENYL)ACETAMIDE

There total 3 articles about (2E)-2-(HYDROXYIMINO)-N-(3-NITROPHENYL)ACETAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

chloral hydrate (302-17-0) + 3-nitro-aniline (99-09-2) → 3-nitroisonitrosoacetanilide (17122-61-1)

Guidance literature:

With hydrogenchloride; hydroxylamine hydrochloride; sodium sulfate; In water; at 35 - 90 ℃; for 2h;

DOI:10.1080/00397910903318591

Reference yield:

chloral hydrate (302-17-0) + water (7732-18-5) + hydroxylamine (7803-49-8) + 3-nitro-aniline (99-09-2) → 3-nitroisonitrosoacetanilide (17122-61-1)

Guidance literature:

Reference yield:

→ 3-nitroisonitrosoacetanilide (17122-61-1)

Guidance literature:

3-Nitro-anilin m. Chloralhydrat u. Hydroxylamin in einer ges. Lsg. v. Na2SO4 in wss. HCl;

upstream raw materials:

chloral hydrate

3-nitro-aniline

water

hydroxylamine

Downstream raw materials:

N-(3-nitrophenyl)acetanilide

1,3-bis(3-nitrophenyl)urea

1,3,5-tris(3-nitrophenyl)-1,3,5-triazinane-2,4,6-trione

4-nitro-1H-indole-2,3-dione

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