3'-Nitroacetanilide

Base Information

Chemical Name:3'-Nitroacetanilide
CAS No.:122-28-1
Molecular Formula:C8H8N2O3
Molecular Weight:180.163
Hs Code.:29242990
European Community (EC) Number:204-532-6
NSC Number:99339,1314
UNII:QGH8S22NBP
DSSTox Substance ID:DTXSID5059539
Nikkaji Number:J96.165E
Wikidata:Q27287255
ChEMBL ID:CHEMBL1568017
Mol file:122-28-1.mol

Synonyms:3-nitroacetanilide

Suppliers and Price of 3'-Nitroacetanilide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
m-Nitroacetanilide
2.5g
$ 60.00

TCI Chemical
3'-Nitroacetanilide >98.0%(GC)
25g
$ 99.00

Sigma-Aldrich
3′-Nitroacetanilide 97%
25g
$ 242.00

Sigma-Aldrich
3′-Nitroacetanilide 97%
5g
$ 56.80

Frontier Specialty Chemicals
3'-Nitroacetanilide 97%
5g
$ 43.00

Frontier Specialty Chemicals
3'-Nitroacetanilide 97%
25g
$ 140.00

Crysdot
N-(3-Nitrophenyl)acetamide 95+%
500g
$ 742.00

Aronis compounds
N-(3-nitrophenyl)acetamide
5mg
$ 15.00

Arctom
N-(3-Nitrophenyl)acetamide 98%
25g
$ 109.00

Arctom
N-(3-Nitrophenyl)acetamide 98%
5g
$ 32.00

Total 44 raw suppliers

Chemical Property of 3'-Nitroacetanilide

Chemical Property:

Appearance/Colour:Beige crystalline to brown powder
Vapor Pressure:6.04E-06mmHg at 25°C
Melting Point:154-158 °C(lit.)
Refractive Index:1.617
Boiling Point:379.004 °C at 760 mmHg
PKA:14.20±0.70(Predicted)
Flash Point:183.015 °C
PSA：74.92000
Density:1.341 g/cm³
LogP:2.14940
Storage Temp.:Store below +30°C.
Solubility.:almost transparency in hot Methanol
XLogP3:1.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:180.05349212
Heavy Atom Count:13
Complexity:212

Purity/Quality:

99% ^*data from raw suppliers

m-Nitroacetanilide ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes:Xi
Statements: 36/37/38-43
Safety Statements: 26-36/37

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)NC1=CC(=CC=C1)[N+](=O)[O-]
Uses m-Nitroacetanilide is a useful building block used in a variety of synthetic applications, such as the preparation of chalcones and N-?chloroamines.

Technology Process of 3'-Nitroacetanilide

There total 44 articles about 3'-Nitroacetanilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 75-36-5
acetyl chloride

: 99-09-2
3-nitro-aniline

: 122-28-1
N-(3-nitrophenyl)acetanilide

Guidance literature:: bismuth(III) oxychloride; In acetonitrile; at 20 ℃; for 0.0833333h;
DOI:10.1016/j.tetlet.2004.07.044

Reference yield: 94.0%

: 141-78-6
ethyl acetate

: 99-09-2
3-nitro-aniline

: 122-28-1
N-(3-nitrophenyl)acetanilide

Guidance literature:: With zinc borohydride pyridine complex; In tetrahydrofuran; for 4h; Heating;

Reference yield: 90.0%

: 64-19-7,77671-22-8
acetic acid

: 99-09-2
3-nitro-aniline

: 122-28-1
N-(3-nitrophenyl)acetanilide

Guidance literature:: With magnesia; In neat (no solvent); at 70 ℃; for 0.5h; chemoselective reaction; Green chemistry;
DOI:10.1016/j.apcata.2013.02.016