1-Chloro-4-(4-methylphenyl)phthalazine

Base Information

Chemical Name:1-Chloro-4-(4-methylphenyl)phthalazine
CAS No.:76972-35-5
Molecular Formula:C15H11ClN2
Molecular Weight:254.719
Hs Code.:2933990090
European Community (EC) Number:821-884-1
DSSTox Substance ID:DTXSID70423343
Wikidata:Q82235543
Mol file:76972-35-5.mol

Synonyms:1-chloro-4-(4-methylphenyl)phthalazine;76972-35-5;1-chloro-4-(p-tolyl)phthalazine;SCHEMBL7904780;DTXSID70423343;SBSCJEDEQMLKJY-UHFFFAOYSA-N;1-chloro-4-(4-tolyl)phthalazine;MFCD00446456;AKOS000116951;EN300-08257;A915332;Z56928634;F9995-0257

Suppliers and Price of 1-Chloro-4-(4-methylphenyl)phthalazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
1-Chloro-4-(4-methylphenyl)phthalazine 95%+
2.500g
$ 447.00

Matrix Scientific
1-Chloro-4-(4-methylphenyl)phthalazine 95%+
1g
$ 208.00

Matrix Scientific
1-Chloro-4-(4-methylphenyl)phthalazine 95%+
5g
$ 677.00

Crysdot
1-Chloro-4-(p-tolyl)phthalazine 97%
5g
$ 631.00

American Custom Chemicals Corporation
1-CHLORO-4-(4-METHYLPHENYL)PHTHALAZINE 95.00%
5G
$ 1210.63

American Custom Chemicals Corporation
1-CHLORO-4-(4-METHYLPHENYL)PHTHALAZINE 95.00%
2.5G
$ 1011.60

American Custom Chemicals Corporation
1-CHLORO-4-(4-METHYLPHENYL)PHTHALAZINE 95.00%
1G
$ 736.12

Alfa Aesar
1-Chloro-4-(4-methylphenyl)phthalazine, 96%
5g
$ 325.00

Alfa Aesar
1-Chloro-4-(4-methylphenyl)phthalazine, 96%
1g
$ 96.90

Alfa Aesar
1-Chloro-4-(4-methylphenyl)phthalazine, 96%
250mg
$ 36.70

Total 12 raw suppliers

Chemical Property of 1-Chloro-4-(4-methylphenyl)phthalazine

Chemical Property:

Melting Point:159-164℃
Boiling Point:450.1 °C at 760 mmHg
Flash Point:258.5 °C
PSA：25.78000
Density:1.251 g/cm³
LogP:4.25860
XLogP3:4.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:254.0610761
Heavy Atom Count:18
Complexity:276

Purity/Quality:

97% ^*data from raw suppliers

1-Chloro-4-(4-methylphenyl)phthalazine 95%+ ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C2=NN=C(C3=CC=CC=C32)Cl

Technology Process of 1-Chloro-4-(4-methylphenyl)phthalazine

There total 4 articles about 1-Chloro-4-(4-methylphenyl)phthalazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 51334-85-1
4-(4-methylphenyl)-1-(2H)-phthalazinone

: 76972-35-5
1-chloro-4-para-tolylphthalazine

Guidance literature:: With trichlorophosphate; for 5h; Heating;
DOI:10.3184/174751914X14116480062198

Reference yield: 64.0%

: 85-55-2
2-(4-toluoyl)benzoic acid

: 76972-35-5
1-chloro-4-para-tolylphthalazine

Guidance literature:: 2-(4-toluoyl)benzoic acid; With hydrazine;

With trichlorophosphate;
DOI:10.1515/HC.2003.9.6.641

Reference yield:

: 1875-48-5
N-aminophthalamide

: 76972-35-5
1-chloro-4-para-tolylphthalazine

Guidance literature:: Multi-step reaction with 2 steps

1: aluminum (III) chloride

2: trichlorophosphate; N,N-dimethyl-aniline / 100 - 105 °C

With aluminum (III) chloride; N,N-dimethyl-aniline; trichlorophosphate;
DOI:10.3762/bjoc.13.20