Technology Process of Benzeneacetic acid, 3-methoxy-5-(phenylmethoxy)-, methyl ester
There total 6 articles about Benzeneacetic acid, 3-methoxy-5-(phenylmethoxy)-, methyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
(3-benzyloxy-5-methoxyphenyl)acetonitrile;
With
potassium hydroxide; ethylene glycol;
at 120 ℃;
With
hydrogenchloride;
In
water;
methyl iodide;
With
potassium carbonate;
In
DMF (N,N-dimethyl-formamide);
at 20 ℃;
for 1h;
- Guidance literature:
-
methyl 2-(3,5-dihydroxyphenyl)acetate; dimethyl sulfate;
With
tetra-(n-butyl)ammonium iodide; potassium carbonate;
In
acetone;
Heating;
benzyl bromide;
With
potassium carbonate;
In
acetone;
Heating;
DOI:10.1016/S0040-4039(00)00030-7
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium carbonate / DMF (N,N-dimethyl-formamide) / 20 °C
1.2: 20 °C
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 - 20 °C
3.1: tributylphosphine; diethylazodicarboxylate / tetrahydrofuran / 20 °C
4.1: potassium hydroxide; ethylene glycol / 120 °C
4.3: 1 h / 20 °C
With
potassium hydroxide; lithium aluminium tetrahydride; tributylphosphine; potassium carbonate; ethylene glycol; diethylazodicarboxylate;
In
tetrahydrofuran; DMF (N,N-dimethyl-formamide);