1,1,1,4,4,4-Hexachlorobut-2-ene

Base Information

• Chemical Name: 1,1,1,4,4,4-Hexachlorobut-2-ene
• CAS No.: 62897-29-4
• Molecular Formula: C4H2Cl6
• Molecular Weight: 262.778
• DSSTox Substance ID: DTXSID70707478
• Mol file: 62897-29-4.mol

Synonyms:1,1,1,4,4,4-Hexachlorobut-2-ene;62897-29-4;DTXSID70707478

Chemical Property of 1,1,1,4,4,4-Hexachlorobut-2-ene

Chemical Property:

• XLogP3: 4.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 261.825816
• Heavy Atom Count: 10
• Complexity: 110

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C(=CC(Cl)(Cl)Cl)C(Cl)(Cl)Cl

Technology Process of 1,1,1,4,4,4-Hexachlorobut-2-ene

There total 3 articles about 1,1,1,4,4,4-Hexachlorobut-2-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bis(dimethylgermyl)methane ruthenium tetracarbonyl (131145-73-8) + chloral (75-87-6) → dodecacarbonyl-triangulo-triruthenium (15243-33-1) + 2,2,4,4-tetramethyl-1,2,4-oxadigermetane (106652-06-6) + 1,1,1,4,4,4-hexachloro-but-2-ene (62897-29-4)

Guidance literature:

In not given;

DOI:10.1016/S0020-1693(00)84821-5

Reference yield:

bis(dimethylgermyl)ethane ruthenium tetracarbonyl (131145-74-9) + chloral (75-87-6) → dodecacarbonyl-triangulo-triruthenium (15243-33-1) + (CH3)2GeCH2CH2Ge(CH3)2O (120926-63-8) + 1,1,1,4,4,4-hexachloro-but-2-ene (62897-29-4)

Guidance literature:

In not given;

DOI:10.1016/S0020-1693(00)84821-5

Reference yield:

1,1,1,4,4-pentachloro-but-3-en-2-ol (18767-25-4) → 1,1,1,4,4,4-hexachloro-but-2-ene (62897-29-4)

Guidance literature:

With phosphorus pentachloride;

upstream raw materials:

1,1,1,4,4-pentachloro-but-3-en-2-ol

bis(dimethylgermyl)methane ruthenium tetracarbonyl

chloral

bis(dimethylgermyl)ethane ruthenium tetracarbonyl

Downstream raw materials:

1,1,4,4-Tetrakis(4-chlor-phenylthio)-1,3-butadien

1,1,4,4-Tetrakis(phenylthio)-1,3-butadien

1,1,4,4-Tetrakis(4-methyl-phenylthio)-1,3-butadien