5-Bromo-2-methoxybenzoyl chloride

Base Information

Chemical Name:5-Bromo-2-methoxybenzoyl chloride
CAS No.:62910-63-8
Molecular Formula:C8H6BrClO2
Molecular Weight:249.491
Hs Code.:
European Community (EC) Number:657-345-0
Mol file:62910-63-8.mol

Synonyms:5-bromo-2-methoxybenzoyl chloride;62910-63-8;SCHEMBL477809;JBDMIOCVPSFJPW-UHFFFAOYSA-N;5-Bromo-2-methoxy-benzoyl chloride;AKOS000296495;BB 0245345;FT-0731333

Suppliers and Price of 5-Bromo-2-methoxybenzoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
5-BROMO-2-METHOXYBENZOYL CHLORIDE AldrichCPR
1ea
$ 57.00

American Custom Chemicals Corporation
5-BROMO-2-METHOXY-BENZOYL CHLORIDE 95.00%
1G
$ 2249.10

American Custom Chemicals Corporation
5-BROMO-2-METHOXY-BENZOYL CHLORIDE 95.00%
5MG
$ 498.91

Alichem
5-BROMO-2-METHOXYBENZOYL CHLORIDE
250mg
$ 480.00

Total 3 raw suppliers

Chemical Property of 5-Bromo-2-methoxybenzoyl chloride

Chemical Property:

Boiling Point:315.0±27.0 °C(Predicted)
PSA：0.00000
Density:1.598±0.06 g/cm3(Predicted)
LogP:0.00000
XLogP3:3.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:247.92397
Heavy Atom Count:12
Complexity:174

Purity/Quality:

99% ^*data from raw suppliers

5-BROMO-2-METHOXYBENZOYL CHLORIDE AldrichCPR ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)Br)C(=O)Cl

Technology Process of 5-Bromo-2-methoxybenzoyl chloride

There total 4 articles about 5-Bromo-2-methoxybenzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 2476-35-9
5-bromo-2-methoxybenzoic acid

: 62910-63-8
5-bromo-2-methoxybenzoyl chloride

Guidance literature:: With oxalyl dichloride; In dichloromethane; N,N-dimethyl-formamide; at -5 ℃; Inert atmosphere;

Reference yield:

: 89-55-4
5-bromosalicyclic acid

: 62910-63-8
5-bromo-2-methoxybenzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / water / 0.5 h / 37 °C / pH 10

1.2: 2.25 h / 80 °C / pH 7 - 10

2.1: N,N-dimethyl-formamide; thionyl chloride / dichloromethane / 0.5 h / 40 °C

With thionyl chloride; N,N-dimethyl-formamide; sodium hydroxide; In dichloromethane; water;

Reference yield:

: 7120-41-4
methyl 5-bromo-2-methoxybenzoate

: 62910-63-8
5-bromo-2-methoxybenzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 5N aq. NaOH / ethanol / 18 h / 22 °C

2: (COCl)2, DMF / CH₂Cl₂ / 3.25 h / 22 °C

With sodium hydroxide; oxalyl dichloride; N,N-dimethyl-formamide; In ethanol; dichloromethane;
DOI:10.1002/(SICI)1099-1344(199609)38:9<863::AID-JLCR895>3.0.CO;2-0