4-Thiomorpholinecarboxylic acid, (2R,4S)-1-[[[[3,5-bis(trifluoromethyl)phenyl]methyl]methylamino]carbonyl ]-2-(4-fluoro-2-methylphenyl)-4-piperidinyl ester

Base Information

Chemical Name:4-Thiomorpholinecarboxylic acid, (2R,4S)-1-[[[[3,5-bis(trifluoromethyl)phenyl]methyl]methylamino]carbonyl ]-2-(4-fluoro-2-methylphenyl)-4-piperidinyl ester
CAS No.:629937-26-4
Molecular Formula:C28H30F7N3O3S
Molecular Weight:621.619
Hs Code.:

4-Thiomorpholinecarboxylic acid,
(2R,4S)-1-[[[[3,5-bis(trifluoromethyl)phenyl]methyl]methylamino]carbonyl
]-2-(4-fluoro-2-methylphenyl)-4-piperidinyl ester

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Thiomorpholinecarboxylic acid, (2R,4S)-1-[[[[3,5-bis(trifluoromethyl)phenyl]methyl]methylamino]carbonyl ]-2-(4-fluoro-2-methylphenyl)-4-piperidinyl ester

Chemical Property:

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Technology Process of 4-Thiomorpholinecarboxylic acid, (2R,4S)-1-[[[[3,5-bis(trifluoromethyl)phenyl]methyl]methylamino]carbonyl ]-2-(4-fluoro-2-methylphenyl)-4-piperidinyl ester

There total 1 articles about 4-Thiomorpholinecarboxylic acid, (2R,4S)-1-[[[[3,5-bis(trifluoromethyl)phenyl]methyl]methylamino]carbonyl ]-2-(4-fluoro-2-methylphenyl)-4-piperidinyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123-90-0
Thiomorpholin

: 629922-66-3
(2R,4S)-1-{N-(3,5-bistrifluoromethylbenzyl)-N-methyl}amino-carbonyl-2-(4-fluoro-2-methylphenyl)-4-hydroxypiperidine

: 530-62-1
1,1'-carbonyldiimidazole

: 629937-26-4
(2R,4S)-1-[N-(3,5-bistrifluoromethylbenzyl)-N-methyl]aminocarbonyl-2-(4-fluoro-2-methylphenyl)-4-thiomorpholinocarbonyloxypiperidine

Guidance literature:: (2R,4S)-1-{N-(3,5-bistrifluoromethylbenzyl)-N-methyl}amino-carbonyl-2-(4-fluoro-2-methylphenyl)-4-hydroxypiperidine; 1,1'-carbonyldiimidazole; In dichloromethane; toluene; at 60 ℃; for 4h;

With methyl iodide; In acetonitrile; at 50 ℃; for 3h;

Thiomorpholin; In toluene; at 70 ℃; for 16h;