p-Tetradecyloxyphenylacetylchloride

Base Information

Chemical Name:p-Tetradecyloxyphenylacetylchloride
CAS No.:63290-16-4
Molecular Formula:C22H35ClO2
Molecular Weight:366.972
Hs Code.:
DSSTox Substance ID:DTXSID60434362
Wikidata:Q82248753

Synonyms:p-tetradecyloxyphenylacetylchloride;63290-16-4;Benzeneacetyl chloride, 4-(tetradecyloxy)-;SCHEMBL9162853;DTXSID60434362;VEBLYBKIDNJSAX-UHFFFAOYSA-N;p-Tetradecyloxyphenylacetyl chloride;p-tetradecyloxy phenylacetyl chloride;4-(Tetradecyloxy)benzeneacetyl chloride

Suppliers and Price of p-Tetradecyloxyphenylacetylchloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of p-Tetradecyloxyphenylacetylchloride

Chemical Property:

XLogP3:9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:16
Exact Mass:366.2325580
Heavy Atom Count:25
Complexity:311

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCCCCCCCCCCOC1=CC=C(C=C1)CC(=O)Cl

Technology Process of p-Tetradecyloxyphenylacetylchloride

There total 6 articles about p-Tetradecyloxyphenylacetylchloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 63290-17-5
(4-tetradecyloxyphenyl)acetic acid

: 63290-16-4
4-(Tetradecyloxy)benzeneacetyl chloride

Guidance literature:: With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; for 18h;
DOI:10.1021/jm00104a002

Reference yield:

: 79-37-8
oxalyl dichloride

: 63290-17-5
(4-tetradecyloxyphenyl)acetic acid

: 63290-16-4
4-(Tetradecyloxy)benzeneacetyl chloride

Guidance literature:: In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 112-71-0
1-Bromotetradecane

: 63290-16-4
4-(Tetradecyloxy)benzeneacetyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / potassium carbonate / acetone / 72 h / Heating

2: 82 percent / aq. KOH / ethanol / 18 h / Heating

3: 99 percent / oxalyl chloride, DMF / CH₂Cl₂ / 18 h

With potassium hydroxide; oxalyl dichloride; potassium carbonate; N,N-dimethyl-formamide; In ethanol; dichloromethane; acetone;
DOI:10.1021/jm00104a002