4-Hydroxyantipyrine glucuronide

Base Information

Chemical Name:4-Hydroxyantipyrine glucuronide
CAS No.:28070-40-8
Molecular Formula:C17H20 N2 O8
Molecular Weight:380.354
Hs Code.:
UNII:RG9U3YZ7HY

Synonyms:4-Hydroxyantipyrine glucuronide;RG9U3YZ7HY;UNII-RG9U3YZ7HY;28070-40-8;beta-D-Glucopyranosiduronic acid, 2,3-dihydro-1,5-dimethyl-3-oxo-2-phenyl-1H-pyrazol-4-yl;OHA-G;4-HYDROXYPHENAZOLE GLUCURONIDE;.BETA.-D-GLUCOPYRANOSIDURONIC ACID, 2,3-DIHYDRO-1,5-DIMETHYL-3-OXO-2-PHENYL-1H-PYRAZOL-4-YL;2,3-DIHYDRO-1,5-DIMETHYL-3-OXO-2-PHENYL-1H-PYRAZOL-4-YL .BETA.-D-GLUCOPYRANOSIDURONIC ACID

Suppliers and Price of 4-Hydroxyantipyrine glucuronide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
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Total 0 raw suppliers

Chemical Property of 4-Hydroxyantipyrine glucuronide

Chemical Property:

XLogP3:0.3
Hydrogen Bond Donor Count:4
Hydrogen Bond Acceptor Count:9
Rotatable Bond Count:4
Exact Mass:380.12196560
Heavy Atom Count:27
Complexity:632

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C(=O)N(N1C)C2=CC=CC=C2)OC3C(C(C(C(O3)C(=O)O)O)O)O
Isomeric SMILES:CC1=C(C(=O)N(N1C)C2=CC=CC=C2)O[C@H]3[C@@H]([C@H]([C@@H]([C@H](O3)C(=O)O)O)O)O

Technology Process of 4-Hydroxyantipyrine glucuronide

There total 3 articles about 4-Hydroxyantipyrine glucuronide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 122505-42-4
Methyl 1'-<4-hydroxy-2,3-dimethyl-1-phenyl-3-pyrazoline-5-one>-2',3',4'-tri-O-acetyl-β-D-glucopyranuronate

: 28070-40-8
4-Hydroxy-antipyrine β-D-glucuronide

Guidance literature:: With sodium hydroxide; In methanol; 1.) 20 deg C, 2 h, 2.) 45 deg C, 6 h;
DOI:10.1002/ardp.19893220605

Reference yield:

: 5426-65-3
4-bromoantipyrine

: 28070-40-8
4-Hydroxy-antipyrine β-D-glucuronide

Guidance literature:: Multi-step reaction with 3 steps

1: 54 percent / aq. KOH / Triton B / 3 h / Heating

2: 69 percent / CdCO₃ / toluene / 3 h / Heating

3: 71 percent / 6M aq. NaOH / methanol / 1.) 20 deg C, 2 h, 2.) 45 deg C, 6 h

With potassium hydroxide; sodium hydroxide; cadmium(II) carbonate; N-benzyl-trimethylammonium hydroxide; In methanol; toluene;
DOI:10.1002/ardp.19893220605

Reference yield:

: 1672-63-5
4-hydroxyantipyrine

: 28070-40-8
4-Hydroxy-antipyrine β-D-glucuronide

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / CdCO₃ / toluene / 3 h / Heating

2: 71 percent / 6M aq. NaOH / methanol / 1.) 20 deg C, 2 h, 2.) 45 deg C, 6 h

With sodium hydroxide; cadmium(II) carbonate; In methanol; toluene;
DOI:10.1002/ardp.19893220605