Methanone, (2,6-dihydroxyphenyl)phenyl-

Base Information

• Chemical Name: Methanone, (2,6-dihydroxyphenyl)phenyl-
• CAS No.: 63411-81-4
• Molecular Formula: C13H10O3
• Molecular Weight: 214.221
• Mol file: 63411-81-4.mol

Synonyms:1-(2,6-dihydroxyphenyl)phenylketone;Methanone,(2,6-dihydroxyphenyl)phenyl;benzoyl-resorcinol;(2,6-Dihydroxyphenyl)(phenyl)methanone;2,6-Dihydroxy-benzophenon;2-benzoylresorcinol;2,6-dihydroxybenzophenone;Phen-1,3-diol,2-benzoyl;

Chemical Property of Methanone, (2,6-dihydroxyphenyl)phenyl-

Chemical Property:

• Melting Point: 135°C
• PSA: 57.53000
• LogP: 2.32880

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methanone, (2,6-dihydroxyphenyl)phenyl-

There total 12 articles about Methanone, (2,6-dihydroxyphenyl)phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

(2,6-dimethoxyphenyl)(phenyl)methanone (25855-75-8) → benzoyl-resorcinol (63411-81-4)

Guidance literature:

With boron tribromide; In dichloromethane; 1.) 0 deg C, 15 min, 2.) room temperature, overnight;

DOI:10.1016/S0223-5234(97)81679-0

Reference yield: 52.0%

2-benzoyl-3-hydroxycyclohex-2-en-1-one (61834-43-3) → benzoyl-resorcinol (63411-81-4)

Guidance literature:

With 4-methylisopropylbenzene; palladium on activated charcoal; for 72h; Heating;

Reference yield:

benzoyl chloride (98-88-4) + recorcinol (108-46-3) → benzoyl-resorcinol (63411-81-4)

Guidance literature:

benzoyl chloride; recorcinol; With aluminum (III) chloride; In diethyl ether; at 90 ℃;

With hydrogenchloride; In water; at 70 ℃; for 0.5h;

DOI:10.1002/ardp.201100279

upstream raw materials:

1-methyl-4-nitrosobenzene

8-Benzoyl-7-hydroxy-4-methylcoumarin

2-benzoyl-3-hydroxycyclohex-2-en-1-one

(2,6-dimethoxyphenyl)(phenyl)methanone

Downstream raw materials:

(2,6-dimethoxyphenyl)(phenyl)methanone

5-Methoxy-4-phenyl-2H-1-benzopyran-2-one

5-hydroxy-4-phenyl-coumarin

Acetic acid 6-(2,3-dibromo-propyl)-2-oxo-3,4-diphenyl-2H-chromen-5-yl ester