Methanone, (2,6-dimethoxyphenyl)phenyl-

Base Information

• Chemical Name: Methanone, (2,6-dimethoxyphenyl)phenyl-
• CAS No.: 25855-75-8
• Molecular Formula: C15H14O3
• Molecular Weight: 242.274
• DSSTox Substance ID: DTXSID50357950
• Nikkaji Number: J337.628A
• Wikidata: Q82138157
• Mol file: 25855-75-8.mol

Synonyms:2,6-dimethoxybenzophenone;25855-75-8;Methanone, (2,6-dimethoxyphenyl)phenyl-;CBMicro_009235;Oprea1_665149;SCHEMBL9467809;DTXSID50357950;YLETYJUVHBZQHL-UHFFFAOYSA-N;SMSF0006370;(2,6-Dimethoxy-phenyl)-phenyl-methanone;BIM-0009167.P001;SR-01000214565;SR-01000214565-1

Chemical Property of Methanone, (2,6-dimethoxyphenyl)phenyl-

Chemical Property:

• XLogP3: 3.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 4
• Exact Mass: 242.094294304
• Heavy Atom Count: 18
• Complexity: 259

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: COC1=C(C(=CC=C1)OC)C(=O)C2=CC=CC=C2

Technology Process of Methanone, (2,6-dimethoxyphenyl)phenyl-

There total 14 articles about Methanone, (2,6-dimethoxyphenyl)phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

1-(benzoyl)piperidine-2,6-dione + (2,6-dimethoxyphenyl)boronic acid (23112-96-1) → (2,6-dimethoxyphenyl)(phenyl)methanone (25855-75-8)

Guidance literature:

With palladium diacetate; sodium carbonate; tricyclohexylphosphine tetrafluoroborate; In 1,4-dioxane; at 120 ℃; for 15h; Inert atmosphere; Schlenk technique;

DOI:10.1021/acs.orglett.9b02961

Reference yield: 90.0%

benzoic acid anhydride (93-97-0) + 1,3-Dimethoxybenzene (151-10-0) → (2,6-dimethoxyphenyl)(phenyl)methanone (25855-75-8) + 2,4-dimethoxybenzophenone (3555-84-8) + benzoic acid (65-85-0,8013-63-6)

Guidance literature:

With Cl^(1-)*C₅H₁₄NO⁽¹⁺⁾*3ZnCl₂; at 120 ℃; for 0.166667h; Microwave irradiation; Green chemistry;

DOI:10.1039/c6ra03551e

Reference yield: 90.0%

benzoyl chloride (98-88-4) + 1,3-Dimethoxybenzene (151-10-0) → (2,6-dimethoxyphenyl)(phenyl)methanone (25855-75-8) + 2,4-dimethoxybenzophenone (3555-84-8)

Guidance literature:

With aluminium dodecatungsten phosphate; at 60 - 70 ℃; for 3.5h;

DOI:10.1016/j.tet.2004.09.049

upstream raw materials:

benzoyl-resorcinol

dimethyl sulfate

1,2,3-trimethoxybenzene

benzoyl chloride

Downstream raw materials:

benzoyl-resorcinol

4-Hydroxy-3-phenyl-benzofuran-2-carboxylic acid methyl ester

(2-Benzoyl-3-hydroxy-phenoxy)-acetic acid methyl ester

N-(3-(2,6-dimethoxyphenyl)-3-hydroxy-3phenylpropylidene)tert.butylamine

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